ethyl N-(5-ethoxycarbonylmethylimino-5-phenyl-1-phthalimidopentane-2-sulfonyl)glycinate

Base Information

Chemical Name:ethyl N-(5-ethoxycarbonylmethylimino-5-phenyl-1-phthalimidopentane-2-sulfonyl)glycinate
CAS No.:1454845-32-9
Molecular Formula:C₂₇H₃₁N₃O₈S
Molecular Weight:557.624
Hs Code.:

Synonyms:ethyl N-(5-ethoxycarbonylmethylimino-5-phenyl-1-phthalimidopentane-2-sulfonyl)glycinate

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Chemical Property of ethyl N-(5-ethoxycarbonylmethylimino-5-phenyl-1-phthalimidopentane-2-sulfonyl)glycinate

Chemical Property:

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Technology Process of ethyl N-(5-ethoxycarbonylmethylimino-5-phenyl-1-phthalimidopentane-2-sulfonyl)glycinate

There total 3 articles about ethyl N-(5-ethoxycarbonylmethylimino-5-phenyl-1-phthalimidopentane-2-sulfonyl)glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1454845-13-6
5-oxo-5-phenyl-1-phthalimidopentane-2-sulfonyl chloride

: 623-33-6
glycine ethyl ester hydrochloride

: 1454845-32-9
ethyl N-(5-ethoxycarbonylmethylimino-5-phenyl-1-phthalimidopentane-2-sulfonyl)glycinate

Guidance literature:: With triethylamine; In dichloromethane; at 35 ℃; Inert atmosphere; Cooling with ice;
DOI:10.1016/j.tet.2013.08.028

Reference yield:

: 5428-09-1
3-phthalimido-1-propene

: 1454845-32-9
ethyl N-(5-ethoxycarbonylmethylimino-5-phenyl-1-phthalimidopentane-2-sulfonyl)glycinate

Guidance literature:: Multi-step reaction with 3 steps

1: dilauryl peroxide / 1,2-dichloro-ethane / Reflux

2: N-chloro-succinimide; hydrogenchloride / water; acetonitrile / 0.25 h / 0 °C

3: triethylamine / dichloromethane / 35 °C / Inert atmosphere; Cooling with ice

With hydrogenchloride; N-chloro-succinimide; dilauryl peroxide; triethylamine; In dichloromethane; water; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1016/j.tet.2013.08.028

Reference yield:

: 226920-42-9
O-ethyl S-4-oxo-4-phenyl-1-phthalimidomethylbutyl dithiocarbonate

: 1454845-32-9
ethyl N-(5-ethoxycarbonylmethylimino-5-phenyl-1-phthalimidopentane-2-sulfonyl)glycinate

Guidance literature:: Multi-step reaction with 2 steps

1: N-chloro-succinimide; hydrogenchloride / water; acetonitrile / 0.25 h / 0 °C

2: triethylamine / dichloromethane / 35 °C / Inert atmosphere; Cooling with ice

With hydrogenchloride; N-chloro-succinimide; triethylamine; In dichloromethane; water; acetonitrile;
DOI:10.1016/j.tet.2013.08.028