Technology Process of C48H83N7O17
There total 13 articles about C48H83N7O17 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
isopropyl alcohol;
at 20 ℃;
for 2h;
DOI:10.1021/ol500022n
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 1 h / 20 °C / pH 8-9
2: palladium 10% on activated carbon; hydrogen / isopropyl alcohol / 2 h / 20 °C
With
palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; isopropyl alcohol;
DOI:10.1021/ol500022n
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium carbonate; thiophenol / acetonitrile / 4 h / 20 °C
2.1: potassium carbonate / acetonitrile / 72 h / 60 °C
3.1: hydrogenchloride / 1,4-dioxane / 5 h / 20 °C
4.1: acetic anhydride; pyridine / 2 h / 20 °C / Inert atmosphere
4.2: 15 h / 20 °C / Inert atmosphere
5.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 1 h / 20 °C / pH 8-9
6.1: palladium 10% on activated carbon; hydrogen / isopropyl alcohol / 2 h / 20 °C
With
pyridine; hydrogenchloride; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; acetic anhydride; potassium carbonate; thiophenol; N-ethyl-N,N-diisopropylamine;
In
1,4-dioxane; dichloromethane; isopropyl alcohol; acetonitrile;
DOI:10.1021/ol500022n