DI-TERT-BUTYL-2-BROMOETHYLIMINODIACETATE

Base Information

• Chemical Name: DI-TERT-BUTYL-2-BROMOETHYLIMINODIACETATE
• CAS No.: 146432-43-1
• Molecular Formula: C14H26BrNO4
• Molecular Weight: 352.269
• Mol file: 146432-43-1.mol

Synonyms:di-tert-butyl 2,2'-((2-bromoethyl)azanediyl)diacetate;2-[bis(t-butyloxycarbonyl-methyl)amino]ethyl bromide;N-(2-BroMoethyl)-N-[2-(1,1-diMethylethoxy)-2-oxoethyl]glycine 1,1-DiMethylethyl Ester;2-[N,N-bis(tert-butyloxycarbonyl-methyl)amino]-1-bromoethane;tert-butyl [(2-bromoethyl)(2-tert-butoxy-2-oxyethyl)amino]acetate;Bis(tert-butyl) N-(2-BroMoethyl)iMinodiacetate;N,N-bis<(tert-butoxycarbonyl)methyl>-2-bromoethylamine;N,N-BIS(T-BUTYL-4-CARBOXYMETHYL)-2-BROMOETHYLAMINE;

Chemical Property of DI-TERT-BUTYL-2-BROMOETHYLIMINODIACETATE

Chemical Property:

• PSA: 55.84000
• LogP: 2.36670
• Solubility.: Acetone, Chloroform, Dichloromethane, Ethyl Acetate, Methanol

Purity/Quality:

99% ^*data from raw suppliers

Di-tert-butyl-2-bromoethyliminodiacetate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Di-tert-butyl-2-bromoethyliminodiacetate (cas# 146432-43-1) is a compound useful in organic synthesis.

Technology Process of DI-TERT-BUTYL-2-BROMOETHYLIMINODIACETATE

There total 6 articles about DI-TERT-BUTYL-2-BROMOETHYLIMINODIACETATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

[tert-Butoxycarbonylmethyl-(2-hydroxy-ethyl)-amino]-acetic acid tert-butyl ester (146432-41-9) → N-(2-bromoethyl)-N-[2-(1,1-dimethylethoxy)-2-oxoethyl]glycine 1,1-dimethylethyl ester (146432-43-1)

Guidance literature:

With N-Bromosuccinimide; triphenylphosphine; In dichloromethane; at 20 ℃; for 3.66667h; Cooling with ice; Inert atmosphere;

Reference yield: 87.0%

bromoacetic acid tert-butyl ester (5292-43-3) + ethanolamine (141-43-5) → N-(2-bromoethyl)-N-[2-(1,1-dimethylethoxy)-2-oxoethyl]glycine 1,1-dimethylethyl ester (146432-43-1)

Guidance literature:

bromoacetic acid tert-butyl ester; ethanolamine; With potassium hydrogencarbonate; In N,N-dimethyl-formamide; at 20 ℃; for 20h;

With N-Bromosuccinimide; triphenylphosphine; In dichloromethane; for 1h;

DOI:10.1016/j.tetlet.2006.06.128

Reference yield: 86.0%

→ N-(2-bromoethyl)-N-[2-(1,1-dimethylethoxy)-2-oxoethyl]glycine 1,1-dimethylethyl ester (146432-43-1)

Guidance literature:

With N-Bromosuccinimide; triphenylphosphine; In dichloromethane; at 0 - 20 ℃; for 4.5h; Cooling with ice;

upstream raw materials:

[tert-Butoxycarbonylmethyl-(2-hydroxy-ethyl)-amino]-acetic acid tert-butyl ester

bromoacetic acid tert-butyl ester

ethanolamine

2-bromoethylamine

Downstream raw materials:

N,N-bis<2-amino>ethyl>-4-nitro-L-phenylalanine benzyl ester

N-<2-amino>ethyl>-4-nitro-L-phenylalanine benzyl ester

N,N-bis[2-[N',N'-bis[(tert-butoxycarbonyl)methyl]amino]ethyl]-L-aspartic acid, benzyl ester

(R)-2-[[2-(bis-tert-butoxycarbonylmethyl-amino)ethyl]-(4-methoxybenzyl)amino]-3-(4-nitrophenyl)-propionic acid methyl ester

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