(1,1'-bis(di(4-methoxyphenyl)phosphino)ferrocene)(p-trifluoromethylphenyl)iodopalladium(II)

Base Information

Chemical Name:(1,1'-bis(di(4-methoxyphenyl)phosphino)ferrocene)(p-trifluoromethylphenyl)iodopalladium(II)
CAS No.:653587-99-6
Molecular Formula:C₄₅H₄₀F₃FeIO₄P₂Pd
Molecular Weight:1052.92
Hs Code.:

Synonyms:(1,1'-bis(di(4-methoxyphenyl)phosphino)ferrocene)(p-trifluoromethylphenyl)iodopalladium(II)

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Chemical Property of (1,1'-bis(di(4-methoxyphenyl)phosphino)ferrocene)(p-trifluoromethylphenyl)iodopalladium(II)

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Technology Process of (1,1'-bis(di(4-methoxyphenyl)phosphino)ferrocene)(p-trifluoromethylphenyl)iodopalladium(II)

There total 1 articles about (1,1'-bis(di(4-methoxyphenyl)phosphino)ferrocene)(p-trifluoromethylphenyl)iodopalladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 70227-89-3
1,1'-bis[bis(4-methoxyphenyl)phosphino]ferrocene

: 653587-97-4
iodo(N,N,N',N'-tetramethylethylenediamine)(p-trifluoromethylphenyl)palladium(II)

: 653587-99-6
(1,1'-bis(di(4-methoxyphenyl)phosphino)ferrocene)(p-trifluoromethylphenyl)iodopalladium(II)

Guidance literature:: In tetrahydrofuran; in glovebox; soln. of Fe complex in THF added to soln. of Pd complex in THF at room temp.; stirred for 5 min; solvent removed partially under reduced pressure; added dropwise at roomtemp. to stirred pentane; ppt. isolated by filtration (glass fritted fu nnel); elem. anal.;
DOI:10.1021/ja037425g

Reference yield:

: 653587-99-6
(1,1'-bis(di(4-methoxyphenyl)phosphino)ferrocene)(p-trifluoromethylphenyl)iodopalladium(II)

: potassium N-methyltoluidide

: 653588-06-8
(1,1'-bis(di(4-methoxyphenyl)phosphino)ferrocene)(p-trifluoromethylphenyl)(methyl(p-tolyl)amide)palladium(II)

Guidance literature:: In tetrahydrofuran-d8; in drybox, in NMR tube; Pd complex dissolved in THF-d8; soln. of ligand salt in THF-d8 added at -78°C; shaken; not isolated; detd. by NMR spectra at -45°C;
DOI:10.1021/ja037425g