cyclo<2,2-dimethyl-β-alanyl-(2S)-2-hydroxy-4-(methylpentanoyl)-(2E,5S,6R,7E)-5-hydroxy-6-methyl-8-phenyl-2,7-octadienoyl-3-chloro-4-<<(9H-fluoren-9-ylmethoxy)carbonyl>amino>-D-phenylalanyl>

Base Information

Chemical Name:cyclo<2,2-dimethyl-β-alanyl-(2S)-2-hydroxy-4-(methylpentanoyl)-(2E,5S,6R,7E)-5-hydroxy-6-methyl-8-phenyl-2,7-octadienoyl-3-chloro-4-<<(9H-fluoren-9-ylmethoxy)carbonyl>amino>-D-phenylalanyl>
CAS No.:240428-80-2
Molecular Formula:C₅₀H₅₄ClN₃O₈
Molecular Weight:860.447
Hs Code.:

cyclo<2,2-dimethyl-β-alanyl-(2S)-2-hydroxy-4-(methylpentanoyl)-(2E,5S,6R,7E)-5-hydroxy-6-methyl-8-phenyl-2,7-octadienoyl-3-chloro-4-<<(9H-fluoren-9-ylmethoxy)carbonyl>amino>-D-phenylalanyl>

Synonyms:cyclo<2,2-dimethyl-β-alanyl-(2S)-2-hydroxy-4-(methylpentanoyl)-(2E,5S,6R,7E)-5-hydroxy-6-methyl-8-phenyl-2,7-octadienoyl-3-chloro-4-<<(9H-fluoren-9-ylmethoxy)carbonyl>amino>-D-phenylalanyl>

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Chemical Property of cyclo<2,2-dimethyl-β-alanyl-(2S)-2-hydroxy-4-(methylpentanoyl)-(2E,5S,6R,7E)-5-hydroxy-6-methyl-8-phenyl-2,7-octadienoyl-3-chloro-4-<<(9H-fluoren-9-ylmethoxy)carbonyl>amino>-D-phenylalanyl>

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Technology Process of cyclo<2,2-dimethyl-β-alanyl-(2S)-2-hydroxy-4-(methylpentanoyl)-(2E,5S,6R,7E)-5-hydroxy-6-methyl-8-phenyl-2,7-octadienoyl-3-chloro-4-<<(9H-fluoren-9-ylmethoxy)carbonyl>amino>-D-phenylalanyl>

There total 1 articles about cyclo<2,2-dimethyl-β-alanyl-(2S)-2-hydroxy-4-(methylpentanoyl)-(2E,5S,6R,7E)-5-hydroxy-6-methyl-8-phenyl-2,7-octadienoyl-3-chloro-4-<<(9H-fluoren-9-ylmethoxy)carbonyl>amino>-D-phenylalanyl> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 240428-79-9
cyclo<2,2-dimethyl-β-alanyl-(2S)-2-hydroxy-4-(methylpentanoyl)-(2E,5S,6R,7E)-5-hydroxy-6-methyl-8-phenyl-2,7-octadienoyl-3-chloro-4-amino-D-phenylalanyl>

: 240428-80-2
cyclo<2,2-dimethyl-β-alanyl-(2S)-2-hydroxy-4-(methylpentanoyl)-(2E,5S,6R,7E)-5-hydroxy-6-methyl-8-phenyl-2,7-octadienoyl-3-chloro-4-<<(9H-fluoren-9-ylmethoxy)carbonyl>amino>-D-phenylalanyl>

Guidance literature:: With sodium hydrogencarbonate; In 1,4-dioxane; water; for 48h; Ambient temperature;
DOI:10.1021/jm980706s

Reference yield: 100.0%

: 240428-80-2
cyclo<2,2-dimethyl-β-alanyl-(2S)-2-hydroxy-4-(methylpentanoyl)-(2E,5S,6R,7E)-5-hydroxy-6-methyl-8-phenyl-2,7-octadienoyl-3-chloro-4-<<(9H-fluoren-9-ylmethoxy)carbonyl>amino>-D-phenylalanyl>

: (2-Chloro-4-{(E)-(3S,10R,16S)-3-isobutyl-6,6-dimethyl-2,5,9,12-tetraoxo-16-[(S)-1-(3-phenyl-oxiranyl)-ethyl]-1,4-dioxa-8,11-diaza-cyclohexadec-13-en-10-ylmethyl}-phenyl)-carbamic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 25 ℃;
DOI:10.1021/jm980706s

Reference yield:

: 240428-80-2
cyclo<2,2-dimethyl-β-alanyl-(2S)-2-hydroxy-4-(methylpentanoyl)-(2E,5S,6R,7E)-5-hydroxy-6-methyl-8-phenyl-2,7-octadienoyl-3-chloro-4-<<(9H-fluoren-9-ylmethoxy)carbonyl>amino>-D-phenylalanyl>

: 240428-96-0
cyclo<2,2-dimethyl-β-alanyl-(2S)-2-hydroxy-4-(methylpentanoyl)-(2E,5S,6S)-5-hydroxy-6-<(2R,3R)-3-phenyloxiranyl>-2-heptenoyl-4-amino-3-chloro-D-phenylalanyl>

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 25 °C

2: 32 percent / piperidine / dimethylformamide / 6 h / Ambient temperature

With piperidine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm980706s