(Cl)C₆H₄CH(OC₂H₅)CH₂CHCH₂

Base Information

• Chemical Name: (Cl)C₆H₄CH(OC₂H₅)CH₂CHCH₂
• CAS No.: 915289-05-3
• Molecular Formula: C₁₂H₁₅ClO
• Molecular Weight: 210.704
• Mol file: 915289-05-3.mol

Synonyms:(Cl)C₆H₄CH(OC₂H₅)CH₂CHCH₂

Chemical Property of (Cl)C₆H₄CH(OC₂H₅)CH₂CHCH₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (Cl)C₆H₄CH(OC₂H₅)CH₂CHCH₂

There total 2 articles about (Cl)C₆H₄CH(OC₂H₅)CH₂CHCH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

ethyl trimethylsilyl ether (1825-62-3) + 2-chloro-benzaldehyde (89-98-5) + allyl-trimethyl-silane (762-72-1) → (Cl)C6H4CH(OC2H5)CH2CHCH2 (915289-05-3)

Guidance literature:

With bismuth(lll) trifluoromethanesulfonate; In dichloromethane; at 0 ℃;

DOI:10.1055/s-2006-948182

Reference yield:

allyltriethoxysilane (2550-04-1) + 2-chloro-benzaldehyde (89-98-5) → (Cl)C6H4CH(OC2H5)CH2CHCH2 (915289-05-3)

Guidance literature:

With chloro-trimethyl-silane; indium(III) chloride; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1016/j.tetlet.2007.11.062

Reference yield:

(Cl)C6H4CH(OC2H5)CH2CHCH2 (915289-05-3) → 1-ethoxy-3-methylindane + 1-ethoxy-3-methylindane + (1-ethoxy-but-3-enyl)benzene (54703-48-9)

Guidance literature:

With potassium bromide; Ni(tmc)Br₂; In N,N-dimethyl-formamide; at 25 ℃; Further Variations:; Catalysts; Product distribution; Electrochemical reaction;

DOI:10.1055/s-2006-948182

upstream raw materials:

ethyl trimethylsilyl ether

2-chloro-benzaldehyde

allyl-trimethyl-silane

allyltriethoxysilane

Downstream raw materials:

(1-ethoxy-but-3-enyl)benzene