2,6-bis-(4-methoxyphenyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

Base Information

Chemical Name:2,6-bis-(4-methoxyphenyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene
CAS No.:1469857-83-7
Molecular Formula:C₂₂H₁₈N₂O₂S
Molecular Weight:374.463
Hs Code.:

Synonyms:2,6-bis-(4-methoxyphenyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

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Chemical Property of 2,6-bis-(4-methoxyphenyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

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Technology Process of 2,6-bis-(4-methoxyphenyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

There total 7 articles about 2,6-bis-(4-methoxyphenyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1469858-53-4
2,6-bis-(4-methoxyphenyl)-4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

: 1469857-83-7
2,6-bis-(4-methoxyphenyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

Guidance literature:: With hydrogenchloride; In methanol; at 100 ℃; for 4h;

Reference yield:

: 1469857-45-1
2-bromo-6-(4-methoxyphenyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

: 1469857-83-7
2,6-bis-(4-methoxyphenyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 80 °C

2: sodium carbonate; bis-triphenylphosphine-palladium(II) chloride / ethanol; toluene / 8 h / 100 °C

3: hydrogenchloride / methanol / 4 h / 100 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; sodium hydride; sodium carbonate; In tetrahydrofuran; methanol; ethanol; toluene; mineral oil;

Reference yield:

: 4181-97-9
phenyl 4-methoxybenzoate

: 1469857-83-7
2,6-bis-(4-methoxyphenyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 8 h / 100 °C

2: hydrazine hydrate; acetic acid / ethanol / 4 h / 100 °C / Inert atmosphere

3: acetic acid; bromine / 12 h / 80 °C

4: sodium hydride / tetrahydrofuran; mineral oil / 0 - 80 °C

5: sodium carbonate; bis-triphenylphosphine-palladium(II) chloride / ethanol; toluene / 8 h / 100 °C

6: hydrogenchloride / methanol / 4 h / 100 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; bromine; sodium hydride; sodium carbonate; hydrazine hydrate; acetic acid; In tetrahydrofuran; methanol; ethanol; toluene; mineral oil;