N-(6-(diethylamino)-9-phenyl-3H-xanthen-3-ylidene)-N-ethylethanaminium chloride

Base Information

Chemical Name:N-(6-(diethylamino)-9-phenyl-3H-xanthen-3-ylidene)-N-ethylethanaminium chloride
CAS No.:13482-21-8
Molecular Formula:C₂₇H₃₁N₂O*Cl
Molecular Weight:435.009
Hs Code.:

Synonyms:N-(6-(diethylamino)-9-phenyl-3H-xanthen-3-ylidene)-N-ethylethanaminium chloride

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Chemical Property of N-(6-(diethylamino)-9-phenyl-3H-xanthen-3-ylidene)-N-ethylethanaminium chloride

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Technology Process of N-(6-(diethylamino)-9-phenyl-3H-xanthen-3-ylidene)-N-ethylethanaminium chloride

There total 4 articles about N-(6-(diethylamino)-9-phenyl-3H-xanthen-3-ylidene)-N-ethylethanaminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1608130-71-7
4-(diethylamino)-2-(3-(diethylamino)phenoxy)benzaldehyde

: 100-58-3
phenylmagnesium bromide

: 13482-21-8
N-(6-(diethylamino)-9-phenyl-3H-xanthen-3-ylidene)-N-ethylethanaminium chloride

Guidance literature:: 4-(diethylamino)-2-(3-(diethylamino)phenoxy)benzaldehyde; phenylmagnesium bromide; In tetrahydrofuran; at -78 - 20 ℃; for 0.5h;

With hydrogenchloride; In tetrahydrofuran; water; at 50 ℃; for 0.25h;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; at 20 ℃; for 0.5h;
DOI:10.1021/acs.joc.5b01746

Reference yield:

: 591-19-5
m-Bromoaniline

: 13482-21-8
N-(6-(diethylamino)-9-phenyl-3H-xanthen-3-ylidene)-N-ethylethanaminium chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetonitrile / 24 h / 80 °C

2.1: trichlorophosphate / 6.5 h / 0 - 20 °C

3.1: potassium carbonate; copper(I) bromide / N,N-dimethyl-formamide / 120 °C

4.1: tetrahydrofuran / 0.5 h / -78 - 20 °C

4.2: 0.25 h / 50 °C

4.3: 0.5 h / 20 °C

With potassium carbonate; copper(I) bromide; trichlorophosphate; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile; 2.1: |Vilsmeier-Haack Formylation / 3.1: |Ullmann Condensation;
DOI:10.1021/acs.joc.5b01746

Reference yield:

: 53142-19-1
3-bromo-bisethyl-aminobenzene

: 13482-21-8
N-(6-(diethylamino)-9-phenyl-3H-xanthen-3-ylidene)-N-ethylethanaminium chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: trichlorophosphate / 6.5 h / 0 - 20 °C

2.1: potassium carbonate; copper(I) bromide / N,N-dimethyl-formamide / 120 °C

3.1: tetrahydrofuran / 0.5 h / -78 - 20 °C

3.2: 0.25 h / 50 °C

3.3: 0.5 h / 20 °C

With potassium carbonate; copper(I) bromide; trichlorophosphate; In tetrahydrofuran; N,N-dimethyl-formamide; 1.1: |Vilsmeier-Haack Formylation / 2.1: |Ullmann Condensation;
DOI:10.1021/acs.joc.5b01746