C₂₃H₃₆O₃Si

Base Information

Chemical Name:C₂₃H₃₆O₃Si
CAS No.:1610729-83-3
Molecular Formula:C₂₃H₃₆O₃Si
Molecular Weight:388.623
Hs Code.:

C<sub>23</sub>H<sub>36</sub>O<sub>3</sub>Si

Synonyms:C₂₃H₃₆O₃Si

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Chemical Property of C₂₃H₃₆O₃Si

Chemical Property:

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Technology Process of C₂₃H₃₆O₃Si

There total 2 articles about C₂₃H₃₆O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1610729-82-2
C₁₇H₂₂O₃

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1610729-83-3
C₂₃H₃₆O₃Si

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 40 ℃; for 0.5h;
DOI:10.1021/jo500795z

Reference yield:

: 5-cyano-5-(1-ethoxyethoxy)-3,7-dimethylocta-2,6-dien-1-yl benzoate

: 1610729-83-3
C₂₃H₃₆O₃Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid; methanol / water / 0.33 h / 20 °C

1.2: 0 °C

1.3: 0.25 h / 0 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / 40 °C

With 1H-imidazole; methanol; toluene-4-sulfonic acid; In water; N,N-dimethyl-formamide; 1.3: |Luche Cerium Reduction;
DOI:10.1021/jo500795z

Reference yield:

: 1610729-83-3
C₂₃H₃₆O₃Si

: 126654-52-2
(E)-5-(3,7-dimethyl-5-oxoocta-2,6-dien-1-yl)-4-hydroxy-6-methoxyisobenzofuran-1(3H)-one

Guidance literature:: Multi-step reaction with 9 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 1 h / -78 °C

2.1: n-butyllithium / tetrahydrofuran / 0.58 h / -78 °C

2.2: 0.58 h / -78 °C

3.1: tetrahydrofuran / 5.5 h / -78 - -40 °C

4.1: trans-bis(triphenylphosphine)palladium dichloride; cesium fluoride / N,N-dimethyl-formamide / 24 h / 85 °C

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.08 h / 0 °C

6.1: silver carbonate / toluene / 3 h / Reflux

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 7 h / 40 °C

8.1: [bis(acetoxy)iodo]benzene; 2-azatricyclo[3.3.1.1^3,7]dec-2-yloxidanyl / dichloromethane / 3.67 h / 20 °C

9.1: 1-penten; dimethylboron bromide / dichloromethane / 1 h / -78 °C

9.2: 1 h / 0 °C

With lithium aluminium tetrahydride; n-butyllithium; trans-bis(triphenylphosphine)palladium dichloride; 2-azatricyclo[3.3.1.1^3,7]dec-2-yloxidanyl; dimethylboron bromide; 1-penten; [bis(acetoxy)iodo]benzene; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; cesium fluoride; silver carbonate; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; 4.1: |Stille Cross Coupling;
DOI:10.1021/jo500795z