4β-[4'-(benzo[c][1,2,5]thiadiazole-4-sulfonamido)benzamide]podophyllotoxin

Base Information

Chemical Name:4β-[4'-(benzo[c][1,2,5]thiadiazole-4-sulfonamido)benzamide]podophyllotoxin
CAS No.:1365699-45-1
Molecular Formula:C₃₅H₃₀N₄O₁₀S₂
Molecular Weight:730.776
Hs Code.:

Synonyms:4β-[4'-(benzo[c][1,2,5]thiadiazole-4-sulfonamido)benzamide]podophyllotoxin

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Chemical Property of 4β-[4'-(benzo[c][1,2,5]thiadiazole-4-sulfonamido)benzamide]podophyllotoxin

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Technology Process of 4β-[4'-(benzo[c][1,2,5]thiadiazole-4-sulfonamido)benzamide]podophyllotoxin

There total 4 articles about 4β-[4'-(benzo[c][1,2,5]thiadiazole-4-sulfonamido)benzamide]podophyllotoxin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1365699-34-8
N₁-((5S,5aS,8aR,9R)-8-oxo-9-(3,4,5-trimethoxyphenyl)-5,5a,6,8,8a,9-hexahydro[1,3]dioxolo[4',5':4,5]benzo[f]isobenzofuran-5-yl)-4-aminobenzamide

: 73713-79-8
benzo(1,2,5)thiadiazole-4-sulfonyl chloride

: 1365699-45-1
4β-[4'-(benzo[c][1,2,5]thiadiazole-4-sulfonamido)benzamide]podophyllotoxin

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1016/j.bmc.2012.01.039

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 1365699-45-1
4β-[4'-(benzo[c][1,2,5]thiadiazole-4-sulfonamido)benzamide]podophyllotoxin

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 3 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate

3: triethylamine / dichloromethane / 3 h / 20 °C

With palladium 10% on activated carbon; hydrogen; triethylamine; In dichloromethane; ethyl acetate;
DOI:10.1016/j.bmc.2012.01.039

Reference yield:

: 1365699-32-6
N₁-((5S,5aS,8aR,9R)-8-oxo-9-(3,4,5-trimethoxyphenyl)-5,5a,6,8,8a,9-hexahydro[1,3]dioxolo[4',5':4,5]benzo[f]isobenzofuran-5-yl)-4-nitrobenzamide

: 1365699-45-1
4β-[4'-(benzo[c][1,2,5]thiadiazole-4-sulfonamido)benzamide]podophyllotoxin

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate

2: triethylamine / dichloromethane / 3 h / 20 °C

With palladium 10% on activated carbon; hydrogen; triethylamine; In dichloromethane; ethyl acetate;
DOI:10.1016/j.bmc.2012.01.039