phenyl 1-pyrenyl sulfoxide

Base Information

Chemical Name:phenyl 1-pyrenyl sulfoxide
CAS No.:1067915-09-6
Molecular Formula:C₂₂H₁₄OS
Molecular Weight:326.419
Hs Code.:

Synonyms:phenyl 1-pyrenyl sulfoxide

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Chemical Property of phenyl 1-pyrenyl sulfoxide

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Technology Process of phenyl 1-pyrenyl sulfoxide

There total 4 articles about phenyl 1-pyrenyl sulfoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 34034-20-3
(1-dihydropyren-3-yl)phenylsulfane

: 1067915-09-6
phenyl 1-pyrenyl sulfoxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 0.666667h;
DOI:10.1021/ja407099a

Reference yield:

: 1714-29-0
1-bromopyrene

: 1067915-09-6
phenyl 1-pyrenyl sulfoxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.25 h / -78 - 20 °C / Inert atmosphere; Cooling with acetone-dry ice

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.67 h / 0 °C

With n-butyllithium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ja407099a

Reference yield:

: 129-00-0
pyrene

: 1067915-09-6
phenyl 1-pyrenyl sulfoxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / dichloromethane / 6 h / 20 °C

2.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 0.25 h / -78 - 20 °C / Inert atmosphere; Cooling with acetone-dry ice

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.67 h / 0 °C

With N-Bromosuccinimide; n-butyllithium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ja407099a