(2R,3R,4S,5S,6R)-2-Azido-6-trityloxymethyl-tetrahydro-pyran-3,4,5-triol

Base Information

Chemical Name:(2R,3R,4S,5S,6R)-2-Azido-6-trityloxymethyl-tetrahydro-pyran-3,4,5-triol
CAS No.:160712-36-7
Molecular Formula:C₂₅H₂₅N₃O₅
Molecular Weight:447.491
Hs Code.:

Synonyms:(2R,3R,4S,5S,6R)-2-Azido-6-trityloxymethyl-tetrahydro-pyran-3,4,5-triol

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Chemical Property of (2R,3R,4S,5S,6R)-2-Azido-6-trityloxymethyl-tetrahydro-pyran-3,4,5-triol

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Technology Process of (2R,3R,4S,5S,6R)-2-Azido-6-trityloxymethyl-tetrahydro-pyran-3,4,5-triol

There total 2 articles about (2R,3R,4S,5S,6R)-2-Azido-6-trityloxymethyl-tetrahydro-pyran-3,4,5-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20379-59-3
D-glucopyranosyl azide

: 76-83-5
trityl chloride

: 160712-36-7
(2R,3R,4S,5S,6R)-2-Azido-6-trityloxymethyl-tetrahydro-pyran-3,4,5-triol

Guidance literature:: With pyridine; at 40 ℃; for 72h;
DOI:10.1055/s-0034-1379473

Reference yield:

: 54325-28-9
6-O-trityl-D-glucopyranose

: 160712-36-7
(2R,3R,4S,5S,6R)-2-Azido-6-trityloxymethyl-tetrahydro-pyran-3,4,5-triol

Guidance literature:: With lithium azide; N,N'-Thionyldiimidazole; Yield given. Multistep reaction; 1) DMF, -30 deg C, 2) DMF, RT;
DOI:10.1016/S0040-4039(00)76700-1