C₁₇H₁₅N₃O₃

Base Information

• Chemical Name: C₁₇H₁₅N₃O₃
• CAS No.: 1350329-27-9
• Molecular Formula: C₁₇H₁₅N₃O₃
• Molecular Weight: 309.324
• Mol file: 1350329-27-9.mol

Synonyms:C₁₇H₁₅N₃O₃

Chemical Property of C₁₇H₁₅N₃O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₇H₁₅N₃O₃

There total 4 articles about C₁₇H₁₅N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

sodium cyanide (773837-37-9) + C16H16N2O4 (1350329-19-9) → C17H15N3O3 (1350329-27-9)

Guidance literature:

C₁₆H₁₆N₂O₄; With dimethyl sulfate; at 60 ℃; for 24h; Inert atmosphere;

sodium cyanide; With sodium hydrogencarbonate; In water; for 0.0833333h;

DOI:10.1039/c1dt11414j

Reference yield:

2-Picolinic acid (98-98-6) → C17H15N3O3 (1350329-27-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: oxalyl dichloride; triethylamine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

4.1: dimethyl sulfate / 24 h / 60 °C / Inert atmosphere

4.2: 0.08 h

With oxalyl dichloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; dimethyl sulfate; In dichloromethane;

DOI:10.1039/c1dt11414j

Reference yield:

pyridine-2-carbonyl chloride (29745-44-6) → C17H15N3O3 (1350329-27-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C

3.1: dimethyl sulfate / 24 h / 60 °C / Inert atmosphere

3.2: 0.08 h

With triethylamine; 3-chloro-benzenecarboperoxoic acid; dimethyl sulfate; In dichloromethane;

DOI:10.1039/c1dt11414j

upstream raw materials:

pyridine-2-carbonyl chloride

2-Picolinic acid

sodium cyanide

C₁₆H₁₆N₂O₄

Downstream raw materials:

C₁₇H₁₇N₃O₃S