Cbz-L-Ala-D-Gln-O-n-C₆H₁₃

Base Information

• Chemical Name: Cbz-L-Ala-D-Gln-O-n-C₆H₁₃
• CAS No.: 79787-36-3
• Molecular Formula: C₂₂H₃₃N₃O₆
• Molecular Weight: 435.521

Synonyms:Cbz-L-Ala-D-Gln-O-n-C₆H₁₃

Chemical Property of Cbz-L-Ala-D-Gln-O-n-C₆H₁₃

Chemical Property:

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Technology Process of Cbz-L-Ala-D-Gln-O-n-C₆H₁₃

There total 3 articles about Cbz-L-Ala-D-Gln-O-n-C₆H₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

D-Glutamin (5959-95-5,26700-71-0) → Cbz-L-Ala-D-Gln-O-n-C6H13 (79787-36-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Et₃N, 2.) dimethylaminopropylamine / 1.) THF, H₂O, 4 deg C, 24 h, 2.) THF, H₂O, 1 h

2: 1.) aq. Cs₂CO₃ / 1.) THF, 2.) DMF, RT, 48 h

With caesium carbonate; triethylamine; 1-amino-3-(dimethylamino)propane;

DOI:10.1021/jm00343a018

Reference yield:

(N-benzyloxycarbonyl)-L-alanine N-hydroxysuccinimide ester (3401-36-3) → Cbz-L-Ala-D-Gln-O-n-C6H13 (79787-36-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Et₃N, 2.) dimethylaminopropylamine / 1.) THF, H₂O, 4 deg C, 24 h, 2.) THF, H₂O, 1 h

2: 1.) aq. Cs₂CO₃ / 1.) THF, 2.) DMF, RT, 48 h

With caesium carbonate; triethylamine; 1-amino-3-(dimethylamino)propane;

DOI:10.1021/jm00343a018

Reference yield:

1-bromo-hexane (111-25-1) + Cbz-L-Ala-D-Gln (74842-54-9) → Cbz-L-Ala-D-Gln-O-n-C6H13 (79787-36-3)

Guidance literature:

With caesium carbonate; Yield given. Multistep reaction; 1.) THF, 2.) DMF, RT, 48 h;

DOI:10.1021/jm00343a018

upstream raw materials:

1-bromo-hexane

Cbz-L-Ala-D-Gln

D-Glutamin

(N-benzyloxycarbonyl)-L-alanine N-hydroxysuccinimide ester

Downstream raw materials:

1-α-O-benzyl-4,6-O-benzylidene-N-acetylmuramyl-L-alanyl-D-glutamine n-hexyl ester

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