Technology Process of Diboron
There total 7 articles about Diboron which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
solid;
byproducts: Ge, LiI; mechanically acivated interaction in vac. vibrating ball mill (molar ratio LiBH4:GeI4=5.9, 70 min), according to: V. V. Volkov, K. G. Myakishev,I. I. Gorbacheva, Izv. Sib. Otd. Akad. Nauk SSSR, Ser. Khim. Nauk, 5 (1 983) No. 12, p. 79; monitored by volumetric anal., IR spectroscopy, chem. anal.;
- Guidance literature:
-
In
solid;
byproducts: Ge, KI; mechanically acivated interaction in vac. vibrating ball mill (molar ratio KBH4:GeI4=3.6, 90 min), according to: V. V. Volkov, K. G. Myakishev, I. I. Gorbacheva, Izv. Sib. Otd. Akad. Nauk SSSR, Ser. Khim. Nauk, 5 (1983) No. 12, p. 79; monitored by volumetric anal., IR spectroscopy, chem. anal.;
Kinetics;
- Guidance literature:
-
In
solid;
byproducts: Ge, NaI; mechanically acivated interaction in vac. vibrating ball mill (molar ratio NaBH4:GeI4=9.8, 150 min), according to: V. V. Volkov, K. G. Myakishev, I. I. Gorbacheva, Izv. Sib. Otd. Akad. Nauk SSSR, Ser. Khim. Nauk, 5 (1983) No. 12, p. 79; monitored by volumetric anal., IR spectroscopy, chem. anal.;
