3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbohydrazide

Base Information

• Chemical Name: 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbohydrazide
• CAS No.: 1024005-20-6
• Molecular Formula: C₁₅H₁₄F₂N₄O
• Molecular Weight: 304.299

Synonyms:3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbohydrazide

Chemical Property of 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbohydrazide

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Technology Process of 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbohydrazide

There total 1 articles about 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

ethyl 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-dien-5-carboxylate (916592-23-9) → 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-diene-5-carbohydrazide (1024005-20-6)

Guidance literature:

With hydrazine; In ethanol; for 8h; Heating / reflux;

Reference yield: 98.0%

3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-diene-5-carbohydrazide (1024005-20-6) + pivaloyl chloride (3282-30-2) → N'-pivaloyl-3-(2,4-diflurophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-diene-5-carbohydrazide (1024003-75-5)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 35 ℃; for 3h;

Reference yield: 65.0%

3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-diene-5-carbohydrazide (1024005-20-6) + pivaloyl chloride (3282-30-2) → 2-(tert-butyl)-5-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2(6),3-dien-3yl]-1,3,4-oxadiazole (1024003-79-9)

Guidance literature:

3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbohydrazide; pivaloyl chloride; With triethylamine; In dichloromethane; at 0 - 35 ℃; for 3h;

With thionyl chloride; In dichloromethane; for 8 - 16h; Heating / reflux;

upstream raw materials:

ethyl 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carboxylate

Downstream raw materials:

2-(tert-butyl)-5-[5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-dien-3yl]-1,3,4-oxadiazole

N'-pivaloyl-3-(2,4-diflurophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbohydrazide

N'-1-hexanoyl-3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-diene-5-carbohydrazide

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