1,2-bisethane

Base Information

• Chemical Name: 1,2-bisethane
• CAS No.: 24413-66-9
• Molecular Formula: C₁₆H₂₀N₂O₂
• Molecular Weight: 272.347

Synonyms:1,2-bisethane

Chemical Property of 1,2-bisethane

Chemical Property:

Purity/Quality:

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Technology Process of 1,2-bisethane

There total 8 articles about 1,2-bisethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1,4-bis(4'-methoxyphenyl)-1,4-diazabuta-1,3-diene (24978-42-5,24764-91-8) → 1,2-bisethane (24413-66-9)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 0 ℃; for 2h; Reflux;

DOI:10.1039/c3cc00063j

Reference yield: 93.0%

Glyoxal (131543-46-9,107-22-2) + 4-methoxy-aniline (104-94-9) → 1,2-bisethane (24413-66-9)

Guidance literature:

In methanol; water;

DOI:10.1016/0040-4020(95)01036-X

Reference yield: 89.0%

(E,E)-N1,N2-bis(4-methoxyphenyl)ethane-1,2-diimine (24978-42-5) → 1,2-bisethane (24413-66-9)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 0 - 20 ℃;

DOI:10.1039/b801684d

upstream raw materials:

4-methoxy-aniline

ethylene dibromide

Glyoxal

(E,E)-N¹,N²-bis(4-methoxyphenyl)ethane-1,2-diimine

Downstream raw materials:

2,5-di(4-methoxyphenyl)-1,2,5-thiadiazolidine-1-oxide

1,3-bis(4-methoxyphenyl)-4,5-dihydroimidazolium chloride

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