4-(1-oxyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethoxy)-3-methoxybenzaldehyde

Base Information

• Chemical Name: 4-(1-oxyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethoxy)-3-methoxybenzaldehyde
• CAS No.: 791591-62-3
• Molecular Formula: C₁₇H₂₂NO₄
• Molecular Weight: 304.366
• Mol file: 791591-62-3.mol

Synonyms:4-(1-oxyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethoxy)-3-methoxybenzaldehyde

Chemical Property of 4-(1-oxyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethoxy)-3-methoxybenzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(1-oxyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethoxy)-3-methoxybenzaldehyde

There total 1 articles about 4-(1-oxyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethoxy)-3-methoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

3-(bromomethyl)-2,5-dihydro-2,2,5,5-tetramethyl-1H-pyrrol-1-oxyl (76893-32-8) + vanillin (121-33-5,8014-42-4) → 4-(1-oxyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethoxy)-3-methoxybenzaldehyde (791591-62-3)

Guidance literature:

With potassium carbonate; In acetone; for 2h; Reflux;

DOI:10.1021/jm801476y

Reference yield: 45.0%

4-(1-oxyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethoxy)-3-methoxybenzaldehyde (791591-62-3) + acetylacetone (123-54-6,81235-32-7) → (1E,6E)-1,7-bis(4-((1-oxyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrol-3-yl)methoxy)-3-methoxyphenyl)hepta-1,6-diene-3,5-dione biradical

Guidance literature:

acetylacetone; With boron trioxide; In ethyl acetate; at 70 ℃; for 3h;

4-(1-oxyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethoxy)-3-methoxybenzaldehyde; With boric acid tributyl ester; In ethyl acetate; at 70 ℃; for 0.5h;

With N-butylamine; In ethyl acetate; at 70 ℃; for 12h;

DOI:10.2174/1871520617666170522124712

Reference yield:

4-(1-oxyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethoxy)-3-methoxybenzaldehyde (791591-62-3) + 2,3-diaminobenzamide (711007-44-2) → C24H29N4O4

Guidance literature:

With toluene-4-sulfonic acid; In toluene; for 8h; Reflux;

DOI:10.1021/jm801476y

upstream raw materials:

3-(bromomethyl)-2,5-dihydro-2,2,5,5-tetramethyl-1H-pyrrol-1-oxyl

vanillin