benzoic acid 1-(ethoxycarbonyl)-1-(3H-imidazol-4-yl-methyl)-4-methyl-2-oxopentyl ester

Base Information

Chemical Name:benzoic acid 1-(ethoxycarbonyl)-1-(3H-imidazol-4-yl-methyl)-4-methyl-2-oxopentyl ester
CAS No.:147314-99-6
Molecular Formula:C₂₀H₂₄N₂O₅
Molecular Weight:372.421
Hs Code.:

Synonyms:benzoic acid 1-(ethoxycarbonyl)-1-(3H-imidazol-4-yl-methyl)-4-methyl-2-oxopentyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzoic acid 1-(ethoxycarbonyl)-1-(3H-imidazol-4-yl-methyl)-4-methyl-2-oxopentyl ester

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Technology Process of benzoic acid 1-(ethoxycarbonyl)-1-(3H-imidazol-4-yl-methyl)-4-methyl-2-oxopentyl ester

There total 3 articles about benzoic acid 1-(ethoxycarbonyl)-1-(3H-imidazol-4-yl-methyl)-4-methyl-2-oxopentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 38585-61-4
4-(chloromethyl)imidazole hydrochloride

: 147314-98-5
benzoic acid 1-(ethoxycarbonyl)-4-methyl-2-oxopentyl ester

: 147314-99-6
benzoic acid 1-(ethoxycarbonyl)-1-(3H-imidazol-4-yl-methyl)-4-methyl-2-oxopentyl ester

Guidance literature:: With sodium ethanolate; In ethanol; for 1.5h;
DOI:10.1021/jo00059a028

Reference yield:

: 34036-16-3
5-methyl-3-oxo-hexanoic acid ethyl ester

: 147314-99-6
benzoic acid 1-(ethoxycarbonyl)-1-(3H-imidazol-4-yl-methyl)-4-methyl-2-oxopentyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaH / 1) benzene, room temperature, 30 min, 2) 3.5 h

2: 65 percent / NaOEt / ethanol / 1.5 h

With sodium ethanolate; sodium hydride; In ethanol;
DOI:10.1021/jo00059a028

Reference yield:

: 94-36-0
dibenzoyl peroxide

: 147314-99-6
benzoic acid 1-(ethoxycarbonyl)-1-(3H-imidazol-4-yl-methyl)-4-methyl-2-oxopentyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaH / 1) benzene, room temperature, 30 min, 2) 3.5 h

2: 65 percent / NaOEt / ethanol / 1.5 h

With sodium ethanolate; sodium hydride; In ethanol;
DOI:10.1021/jo00059a028