methyl 1-{4-chloro-3-[1-(4-ethyloxyphenyl)ethyl]phenyl}-α/β-D-glucopyranoside

Base Information

Chemical Name:methyl 1-{4-chloro-3-[1-(4-ethyloxyphenyl)ethyl]phenyl}-α/β-D-glucopyranoside
CAS No.:1318794-46-5
Molecular Formula:C₂₃H₂₉ClO₇
Molecular Weight:452.932
Hs Code.:

Synonyms:methyl 1-{4-chloro-3-[1-(4-ethyloxyphenyl)ethyl]phenyl}-α/β-D-glucopyranoside

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Chemical Property of methyl 1-{4-chloro-3-[1-(4-ethyloxyphenyl)ethyl]phenyl}-α/β-D-glucopyranoside

Chemical Property:

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Technology Process of methyl 1-{4-chloro-3-[1-(4-ethyloxyphenyl)ethyl]phenyl}-α/β-D-glucopyranoside

There total 8 articles about methyl 1-{4-chloro-3-[1-(4-ethyloxyphenyl)ethyl]phenyl}-α/β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 461432-22-4
(5-bromo-2-chlorophenyl)(4-ethyloxyphenyl)methanone

: 1318794-46-5
methyl 1-{4-chloro-3-[1-(4-ethyloxyphenyl)ethyl]phenyl}-α/β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / 1 h / 20 °C / Cooling with ice

1.2: pH 3 - 4 / Cooling with ice

2.1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 20 °C

3.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Sealed flask

3.2: 1 h

4.1: methanesulfonic acid / toluene; tetrahydrofuran / 20 °C

With triethylsilane; n-butyllithium; methanesulfonic acid; boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 67-56-1
methanol

: C₃₄H₅₉ClO₇Si₄

: 1318794-46-5
methyl 1-{4-chloro-3-[1-(4-ethyloxyphenyl)ethyl]phenyl}-α/β-D-glucopyranoside

Guidance literature:: With methanesulfonic acid; In tetrahydrofuran; toluene; at 20 ℃;

Reference yield:

: 67-56-1
methanol

: 1318794-45-4
1-(5-bromo-2-chlorophenyl)-1-(4-ethyloxyphenyl)ethane

: 32469-28-6,55515-28-1,55515-29-2,32384-65-9
(3R,4S,5R,6R)-3,4,5-tris((trimethylsilyl)oxy)-6-(((trimethylsilyl)oxy)methyl)tetrahydro-2H-pyran-2-one

: 1318794-46-5
methyl 1-{4-chloro-3-[1-(4-ethyloxyphenyl)ethyl]phenyl}-α/β-D-glucopyranoside

Guidance literature:: 1-(5-bromo-2-chlorophenyl)-1-(4-ethyloxyphenyl)ethane; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h; Cooling with acetone-dry ice;

(3R,4S,5R,6R)-3,4,5-tris((trimethylsilyl)oxy)-6-(((trimethylsilyl)oxy)methyl)tetrahydro-2H-pyran-2-one; In tetrahydrofuran; toluene; at -78 ℃; for 1h;

methanol; With methanesulfonic acid; at -78 - 20 ℃;