3-(4-bromophenyl)-4-methyl-5-ethoxycarbonyl-1,3-thiazolium hexafluorophosphate

Base Information

Chemical Name:3-(4-bromophenyl)-4-methyl-5-ethoxycarbonyl-1,3-thiazolium hexafluorophosphate
CAS No.:1268494-69-4
Molecular Formula:C₁₃H₁₃BrNO₂S*F₆P
Molecular Weight:472.186
Hs Code.:

Synonyms:3-(4-bromophenyl)-4-methyl-5-ethoxycarbonyl-1,3-thiazolium hexafluorophosphate

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Chemical Property of 3-(4-bromophenyl)-4-methyl-5-ethoxycarbonyl-1,3-thiazolium hexafluorophosphate

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Technology Process of 3-(4-bromophenyl)-4-methyl-5-ethoxycarbonyl-1,3-thiazolium hexafluorophosphate

There total 3 articles about 3-(4-bromophenyl)-4-methyl-5-ethoxycarbonyl-1,3-thiazolium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 51656-11-2
3-(4-bromophenyl)-4-methyl-5-ethoxycarbonyl-3H-thiazole-2-thione

: 1268494-69-4
3-(4-bromophenyl)-4-methyl-5-ethoxycarbonyl-1,3-thiazolium hexafluorophosphate

Guidance literature:: 3-(4-bromophenyl)-4-methyl-5-ethoxycarbonyl-3H-thiazole-2-thione; With dihydrogen peroxide; acetic acid; In water; at 20 ℃; for 2.5h;

With hexafluorophosphoric acid; In water;
DOI:10.1080/10426501003767110

Reference yield:

: 609-15-4
ethyl 2-chloro-3-oxo-butyrate

: 1268494-69-4
3-(4-bromophenyl)-4-methyl-5-ethoxycarbonyl-1,3-thiazolium hexafluorophosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / dimethyl sulfoxide / 1 h / 0 - 20 °C

1.2: 1 h / 0 - 20 °C

1.3: 1 h / Reflux

2.1: dihydrogen peroxide; acetic acid / water / 2.5 h / 20 °C

With dihydrogen peroxide; acetic acid; sodium hydroxide; In water; dimethyl sulfoxide;
DOI:10.1080/10426501003767110

Reference yield:

: 106-40-1
4-bromo-aniline

: 1268494-69-4
3-(4-bromophenyl)-4-methyl-5-ethoxycarbonyl-1,3-thiazolium hexafluorophosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / dimethyl sulfoxide / 1 h / 0 - 20 °C

1.2: 1 h / 0 - 20 °C

1.3: 1 h / Reflux

2.1: dihydrogen peroxide; acetic acid / water / 2.5 h / 20 °C

With dihydrogen peroxide; acetic acid; sodium hydroxide; In water; dimethyl sulfoxide;
DOI:10.1080/10426501003767110