1,1-Diallyl-2,5-bis-(chloromethyl-dimethyl-silanyl)-3,4-diphenyl-1H-silole

Base Information

Chemical Name:1,1-Diallyl-2,5-bis-(chloromethyl-dimethyl-silanyl)-3,4-diphenyl-1H-silole
CAS No.:213009-78-0
Molecular Formula:C₂₈H₃₆Cl₂Si₃
Molecular Weight:527.756
Hs Code.:

Synonyms:1,1-Diallyl-2,5-bis-(chloromethyl-dimethyl-silanyl)-3,4-diphenyl-1H-silole

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Chemical Property of 1,1-Diallyl-2,5-bis-(chloromethyl-dimethyl-silanyl)-3,4-diphenyl-1H-silole

Chemical Property:

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Technology Process of 1,1-Diallyl-2,5-bis-(chloromethyl-dimethyl-silanyl)-3,4-diphenyl-1H-silole

There total 1 articles about 1,1-Diallyl-2,5-bis-(chloromethyl-dimethyl-silanyl)-3,4-diphenyl-1H-silole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1719-57-9
Chloro(chloromethyl)dimethylsilane

: 197172-16-0
di-phenylethynyl-diallylsilane

: 213009-78-0
1,1-Diallyl-2,5-bis-(chloromethyl-dimethyl-silanyl)-3,4-diphenyl-1H-silole

Guidance literature:: With LiC₁₀H₈; Yield given. Multistep reaction; 1.) THF, room temperature, 3 h, 2.) -70 deg C, 15 min, 3.) room temperature;
DOI:10.1016/S0040-4020(98)00620-6

Reference yield: 81.0%

: 213009-78-0
1,1-Diallyl-2,5-bis-(chloromethyl-dimethyl-silanyl)-3,4-diphenyl-1H-silole

: 1,1-Diallyl-2,5-bis-(iodomethyl-dimethyl-silanyl)-3,4-diphenyl-1H-silole

Guidance literature:: With sodium iodide; In butanone; for 24h; Heating;
DOI:10.1016/S0040-4020(98)00620-6

Reference yield:

: 213009-78-0
1,1-Diallyl-2,5-bis-(chloromethyl-dimethyl-silanyl)-3,4-diphenyl-1H-silole

: 3a-Allyl-8,8-dimethyl-1,2-diphenyl-3-trimethylsilanyl-3a,4,5,6,7,8-hexahydro-3a,8-disila-azulene

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / NaI / butan-2-one / 24 h / Heating

2: 33 percent / Bu₃SnH, AIBN / benzene / 14 h / Heating

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium iodide; In butanone; benzene;
DOI:10.1016/S0040-4020(98)00620-6