(R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-en-1-yl trifluoromethanesulfonate

Base Information

Chemical Name:(R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-en-1-yl trifluoromethanesulfonate
CAS No.:730958-86-8
Molecular Formula:C₁₁H₁₅F₃O₃S
Molecular Weight:284.3
Hs Code.:

Synonyms:(R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-en-1-yl trifluoromethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-en-1-yl trifluoromethanesulfonate

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Technology Process of (R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-en-1-yl trifluoromethanesulfonate

There total 1 articles about (R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-en-1-yl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 6485-40-1,2244-16-8
(R)-Carvone

: 730958-86-8
(R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-en-1-yl trifluoromethanesulfonate

Guidance literature:: (R)-Carvone; With L-Selectride; In tetrahydrofuran; at -78 ℃; for 1h;

N,N-phenylbistrifluoromethane-sulfonimide; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1021/ol049780x

Reference yield: 91.0%

: 730958-86-8
(R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-en-1-yl trifluoromethanesulfonate

: 730958-83-5
3-(diethylcarbamoyl)-1-methyl-1H-indol-2-ylboronic acid

: 730958-87-9
(R)-N,N-diethyl-1-methyl-2-(2-methyl-5-(prop-1-en-2-yl)cyclohex-1-enyl)-1H-indole-3-carboxamide

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 100 ℃; for 12h;
DOI:10.1021/ol049780x

Reference yield: 66.0%

: 1-(4'-phenylphenyl)pent-1-yne

: 730958-86-8
(R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-en-1-yl trifluoromethanesulfonate

: (R,E)-4-(1-(2-methyl-5-(prop-1-en-2-yl)cyclohex-1-en-1-yl)pent-1-en-1-yl)-1,1'-biphenyl

Guidance literature:: 1-(4'-phenylphenyl)pent-1-yne; With (S)-(+)-5,5’-bis[di(3,5-di-tert-butyl-4-methoxyphenyl)phosphino]-4,4’-bi-1,3-benzodioxole; copper(l) iodide; Dimethylphenylsilane; sodium trimethylsilanolate; In tetrahydrofuran; for 0.0333333h; Inert atmosphere; Glovebox;

With Pd(cinnamyl)(dppbz)(Cl); In tetrahydrofuran; Inert atmosphere; Glovebox;

(R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-en-1-yl trifluoromethanesulfonate; In tetrahydrofuran; at 45 ℃; for 18h; stereoselective reaction; Sealed tube;
DOI:10.1021/acs.orglett.1c03324