LITHIUM TRIMETHYLSILANOLATE

Base Information

• Chemical Name: LITHIUM TRIMETHYLSILANOLATE
• CAS No.: 2004-14-0
• Molecular Formula: C3H10 O Si . Li
• Molecular Weight: 96.1304
• Hs Code.: 29310099
• Mol file: 2004-14-0.mol

Synonyms:Lithium,(trimethylsiloxy)- (7CI); Lithium trimethylsilanolate; Lithiumtrimethylsiloxide; Trimethylsiloxylithium

Chemical Property of LITHIUM TRIMETHYLSILANOLATE

Chemical Property:

• Vapor Pressure: 24.12 psi ( 55 °C)
• Boiling Point: 75°Cat760mmHg
• Flash Point: °C
• PSA: 23.06000
• Density: 0.81g/cm³
• LogP: 1.25180

Purity/Quality:

97% ^*data from raw suppliers

Lithium trimethylsilanolate 95% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C,T
• Statements: 34-40-23/24/25
• Safety Statements: 26-28-36/37/39-45-27-16

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of LITHIUM TRIMETHYLSILANOLATE

There total 20 articles about LITHIUM TRIMETHYLSILANOLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

lithium (trimethylsilyl)tetramethylcyclopentadienide + formaldehyd (50-00-0,30525-89-4,61233-19-0) → lithium; (1,2,3,5-tetramethyl-4-trimethylsilanyl-cyclopenta-2,4-dienyl)-methanolate + lithium; (1,2,3,4-tetramethyl-5-trimethylsilanyl-cyclopenta-2,4-dienyl)-methanolate + 1,2,3,4-tetramethylfulvene (76089-59-3) + lithium trimethylsilanolate (2004-14-0)

Guidance literature:

lithium (trimethylsilyl)tetramethylcyclopentadienide; formaldehyd; In tetrahydrofuran; at -20 ℃; for 1h;

In tetrahydrofuran; at 20 ℃;

DOI:10.1007/s11172-005-0095-9

Reference yield:

2,2-Dimethylpropionyltrimethylsilylphosphan → 2,2-dimethylpropylidynephosphine (78129-68-7) + lithium trimethylsilanolate (2004-14-0)

Guidance literature:

With methyllithium; In diethyl ether; 1.) -30 deg C; 2.) room temp., 15 min;

Reference yield:

tert-butylperoxytrimethylsilane (3965-63-7) + (2-methylpropyl)lithium (920-36-5,90269-51-5) → 2,5-dimethylhexane (592-13-2) + 1-(1,1-dimethylethoxy)-2-methylpropane (33021-02-2) + lithium trimethylsilanolate (2004-14-0) + lithium tert-butoxide (1907-33-1)

Guidance literature:

In benzene; Further byproducts given;

upstream raw materials:

n-butyllithium

tert-butylperoxytrimethylsilane

bis-trimethylsilanyl peroxide

(2-methylpropyl)lithium

Downstream raw materials:

Hexamethyldisiloxane

octamethyltrisiloxabe

vinyltris(trimethylsiloxy)silane

1,1-dichloro-3,3,3-trimethyl-1-vinyldisiloxane

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