C₁₇H₁₄ClNO₂

Base Information

Chemical Name:C₁₇H₁₄ClNO₂
CAS No.:1584221-42-0
Molecular Formula:C₁₇H₁₄ClNO₂
Molecular Weight:299.757
Hs Code.:

C<sub>17</sub>H<sub>14</sub>ClNO<sub>2</sub>

Synonyms:C₁₇H₁₄ClNO₂

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Chemical Property of C₁₇H₁₄ClNO₂

Chemical Property:

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Technology Process of C₁₇H₁₄ClNO₂

There total 3 articles about C₁₇H₁₄ClNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 98081-84-6
6-chloro-2-methoxycarbonylindole

: 1584221-42-0
C₁₇H₁₄ClNO₂

Guidance literature:: 6-chloro-2-methoxycarbonylindole; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.333333h;

benzyl bromide; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 1h;
DOI:10.1016/j.tet.2013.11.084

Reference yield:

: 98081-76-6
C₁₀H₈ClN₃O₂

: 1584221-42-0
C₁₇H₁₄ClNO₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: 5,5-dimethyl-1,3-cyclohexadiene / 1 h / Reflux; Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 0 °C

2.2: 1 h / 0 - 20 °C

With sodium hydride; In 5,5-dimethyl-1,3-cyclohexadiene; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.tet.2013.11.084

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 1584221-42-0
C₁₇H₁₄ClNO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium methylate / methanol / 3 h / -10 °C

2.1: 5,5-dimethyl-1,3-cyclohexadiene / 1 h / Reflux; Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 0 °C

3.2: 1 h / 0 - 20 °C

With sodium methylate; sodium hydride; In methanol; 5,5-dimethyl-1,3-cyclohexadiene; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.tet.2013.11.084