tert-butyl((2R,3S,4S,5S,6R)-2-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-6-((methoxymethoxy)methyl)-4-methylphenyl)-6-((S)-5,5-dibromo-3-methylpent-4-enyl)-3,5-dimethyltetrahydro-2H-pyran-4-yloxy)dimethylsilane

Base Information

Chemical Name:tert-butyl((2R,3S,4S,5S,6R)-2-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-6-((methoxymethoxy)methyl)-4-methylphenyl)-6-((S)-5,5-dibromo-3-methylpent-4-enyl)-3,5-dimethyltetrahydro-2H-pyran-4-yloxy)dimethylsilane
CAS No.:1054608-70-6
Molecular Formula:C₃₇H₆₆Br₂O₇Si₂
Molecular Weight:838.906
Hs Code.:

tert-butyl((2R,3S,4S,5S,6R)-2-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-6-((methoxymethoxy)methyl)-4-methylphenyl)-6-((S)-5,5-dibromo-3-methylpent-4-enyl)-3,5-dimethyltetrahydro-2H-pyran-4-yloxy)dimethylsilane

Synonyms:tert-butyl((2R,3S,4S,5S,6R)-2-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-6-((methoxymethoxy)methyl)-4-methylphenyl)-6-((S)-5,5-dibromo-3-methylpent-4-enyl)-3,5-dimethyltetrahydro-2H-pyran-4-yloxy)dimethylsilane

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Chemical Property of tert-butyl((2R,3S,4S,5S,6R)-2-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-6-((methoxymethoxy)methyl)-4-methylphenyl)-6-((S)-5,5-dibromo-3-methylpent-4-enyl)-3,5-dimethyltetrahydro-2H-pyran-4-yloxy)dimethylsilane

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Technology Process of tert-butyl((2R,3S,4S,5S,6R)-2-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-6-((methoxymethoxy)methyl)-4-methylphenyl)-6-((S)-5,5-dibromo-3-methylpent-4-enyl)-3,5-dimethyltetrahydro-2H-pyran-4-yloxy)dimethylsilane

There total 1 articles about tert-butyl((2R,3S,4S,5S,6R)-2-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-6-((methoxymethoxy)methyl)-4-methylphenyl)-6-((S)-5,5-dibromo-3-methylpent-4-enyl)-3,5-dimethyltetrahydro-2H-pyran-4-yloxy)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 558-13-4
carbon tetrabromide

: 1054608-46-6
C₃₆H₆₆O₈Si₂

: 1054608-70-6
tert-butyl((2R,3S,4S,5S,6R)-2-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-6-((methoxymethoxy)methyl)-4-methylphenyl)-6-((S)-5,5-dibromo-3-methylpent-4-enyl)-3,5-dimethyltetrahydro-2H-pyran-4-yloxy)dimethylsilane

Guidance literature:: carbon tetrabromide; With triphenylphosphine; zinc; In dichloromethane; for 12h; Inert atmosphere;

C₃₆H₆₆O₈Si₂; In dichloromethane; for 3h; Inert atmosphere;
DOI:10.1021/ol801499s

Reference yield: 98.0%

: 1054608-70-6
tert-butyl((2R,3S,4S,5S,6R)-2-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-6-((methoxymethoxy)methyl)-4-methylphenyl)-6-((S)-5,5-dibromo-3-methylpent-4-enyl)-3,5-dimethyltetrahydro-2H-pyran-4-yloxy)dimethylsilane

: 74-88-4
methyl iodide

: 1054608-48-8
tert-butyl((2R,3S,4S,5S,6R)-2-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-6-((methoxymethoxy)methyl)-4-methylphenyl)-3,5-dimethyl-6-((S)-3-methylhex-4-ynyl)tetrahydro-2H-pyran-4-yloxy)dimethylsilane

Guidance literature:: tert-butyl((2R,3S,4S,5S,6R)-2-(2-(tert-butyldimethylsilyloxy)-3,5-dimethoxy-6-((methoxymethoxy)methyl)-4-methylphenyl)-6-((S)-5,5-dibromo-3-methylpent-4-enyl)-3,5-dimethyltetrahydro-2H-pyran-4-yloxy)dimethylsilane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol801499s