N₂-dimethylaminomethylene-O₆-(2,4,6-triisopropylbenzenesulfonyl)-2'-O-methyl-3',5'-O-di-tert-butylsilanediylguanosine

Base Information

• Chemical Name: N₂-dimethylaminomethylene-O₆-(2,4,6-triisopropylbenzenesulfonyl)-2'-O-methyl-3',5'-O-di-tert-butylsilanediylguanosine
• CAS No.: 1207452-00-3
• Molecular Formula: C₃₇H₅₈N₆O₇SSi
• Molecular Weight: 759.055

Synonyms:N₂-dimethylaminomethylene-O₆-(2,4,6-triisopropylbenzenesulfonyl)-2'-O-methyl-3',5'-O-di-tert-butylsilanediylguanosine

Chemical Property of N₂-dimethylaminomethylene-O₆-(2,4,6-triisopropylbenzenesulfonyl)-2'-O-methyl-3',5'-O-di-tert-butylsilanediylguanosine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of N₂-dimethylaminomethylene-O₆-(2,4,6-triisopropylbenzenesulfonyl)-2'-O-methyl-3',5'-O-di-tert-butylsilanediylguanosine

There total 1 articles about N₂-dimethylaminomethylene-O₆-(2,4,6-triisopropylbenzenesulfonyl)-2'-O-methyl-3',5'-O-di-tert-butylsilanediylguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

N2-dimethylaminomethylene-O6-(2,4,6-triisopropylbenzenesulfonyl)-3',5'-O-di-tert-butylsilanediylguanosine (1207451-99-7) + methyl iodide (74-88-4) → N2-dimethylaminomethylene-O6-(2,4,6-triisopropylbenzenesulfonyl)-2'-O-methyl-3',5'-O-di-tert-butylsilanediylguanosine (1207452-00-3)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

DOI:10.1016/j.bmcl.2009.11.016

upstream raw materials:

N₂-dimethylaminomethylene-O₆-(2,4,6-triisopropylbenzenesulfonyl)-3',5'-O-di-tert-butylsilanediylguanosine

methyl iodide

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