3-amino-2-phenylamino-7-benzyl-5,6,7,8-tetrahydropyrido[4′,3':4,5]thieno[2,3-d]pyrimidin-4(3H)-one

Base Information

Chemical Name:3-amino-2-phenylamino-7-benzyl-5,6,7,8-tetrahydropyrido[4′,3':4,5]thieno[2,3-d]pyrimidin-4(3H)-one
CAS No.:893683-63-1
Molecular Formula:C₂₂H₂₁N₅OS
Molecular Weight:403.508
Hs Code.:

Synonyms:3-amino-2-phenylamino-7-benzyl-5,6,7,8-tetrahydropyrido[4′,3':4,5]thieno[2,3-d]pyrimidin-4(3H)-one

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Chemical Property of 3-amino-2-phenylamino-7-benzyl-5,6,7,8-tetrahydropyrido[4′,3':4,5]thieno[2,3-d]pyrimidin-4(3H)-one

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Technology Process of 3-amino-2-phenylamino-7-benzyl-5,6,7,8-tetrahydropyrido[4′,3':4,5]thieno[2,3-d]pyrimidin-4(3H)-one

There total 5 articles about 3-amino-2-phenylamino-7-benzyl-5,6,7,8-tetrahydropyrido[4′,3':4,5]thieno[2,3-d]pyrimidin-4(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1340480-83-2
C₂₄H₂₃N₃O₂S

: 893683-63-1
3-amino-2-phenylamino-7-benzyl-5,6,7,8-tetrahydropyrido[4′,3':4,5]thieno[2,3-d]pyrimidin-4(3H)-one

Guidance literature:: With hydrazine hydrate; In acetonitrile; at 20 ℃;
DOI:10.1016/j.molstruc.2018.11.091

Reference yield: 32.0%

: 102609-56-3
2-(3-Phenyl-thioureido)-6-benzyl-4,5,6,7-tetrahydro-thieno<2,3-c>pyridin-3-carbonsaeureethylester

: 893683-63-1
3-amino-2-phenylamino-7-benzyl-5,6,7,8-tetrahydropyrido[4′,3':4,5]thieno[2,3-d]pyrimidin-4(3H)-one

Guidance literature:: With hydrazine hydrate; In ethanol; Reflux;
DOI:10.3390/molecules15063932

Reference yield:

: 3612-20-2
1-phenylmethyl-4-piperidone

: 893683-63-1
3-amino-2-phenylamino-7-benzyl-5,6,7,8-tetrahydropyrido[4′,3':4,5]thieno[2,3-d]pyrimidin-4(3H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; sulfur / ethanol / 0.67 h / 60 °C / Cooling with ice

2: triethylamine / hexachloroethane; acetonitrile / 20 °C

3: dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

4: hydrazine hydrate / acetonitrile / 20 °C

With sulfur; hydrazine hydrate; triethylamine; In ethanol; dichloromethane; hexachloroethane; acetonitrile; 1: |Gewald Aminoheterocycles Synthesis / 3: |Aza-Wittig Reaction;
DOI:10.1016/j.molstruc.2018.11.091