Technology Process of methyl 3-t-butyl-4-methoxy-5-methylsulfonyl benzoate
There total 5 articles about methyl 3-t-butyl-4-methoxy-5-methylsulfonyl benzoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
chloroform;
at 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: methanesulfonic acid / 16 h / 70 °C
1.2: 3 h / 50 °C
2.1: N-iodo-succinimide; trifluorormethanesulfonic acid / methanol; dichloromethane / 0.25 h / 20 °C
3.1: zinc / [2,2]bipyridinyl; nickel dibromide / N,N-dimethyl-formamide / 1 h / 130 °C
4.1: potassium carbonate / N,N-dimethyl-formamide / 20 h / 20 °C
5.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 3 h / 20 °C
With
N-iodo-succinimide; methanesulfonic acid; trifluorormethanesulfonic acid; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; zinc;
[2,2]bipyridinyl; nickel dibromide;
In
methanol; dichloromethane; chloroform; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-iodo-succinimide; trifluorormethanesulfonic acid / methanol; dichloromethane / 0.25 h / 20 °C
2: zinc / [2,2]bipyridinyl; nickel dibromide / N,N-dimethyl-formamide / 1 h / 130 °C
3: potassium carbonate / N,N-dimethyl-formamide / 20 h / 20 °C
4: 3-chloro-benzenecarboperoxoic acid / chloroform / 3 h / 20 °C
With
N-iodo-succinimide; trifluorormethanesulfonic acid; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; zinc;
[2,2]bipyridinyl; nickel dibromide;
In
methanol; dichloromethane; chloroform; N,N-dimethyl-formamide;
