tris(tetrahydrofurane)triiodidodysprosium(III)

Base Information

Chemical Name:tris(tetrahydrofurane)triiodidodysprosium(III)
CAS No.:279221-53-3
Molecular Formula:C₁₂H₂₄DyI₃O₃
Molecular Weight:759.534
Hs Code.:

Synonyms:tris(tetrahydrofurane)triiodidodysprosium(III)

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Chemical Property of tris(tetrahydrofurane)triiodidodysprosium(III)

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Technology Process of tris(tetrahydrofurane)triiodidodysprosium(III)

There total 1 articles about tris(tetrahydrofurane)triiodidodysprosium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: dysprosium(II) iodide

: 7732-18-5
water

: 100-47-0
benzonitrile

: 821780-85-2
DyI₃(benzonitrile)4

: 279221-53-3
tris(tetrahydrofurane)triiodidodysprosium(III)

: Dy⁽³⁺⁾*I^(1-)*2OH^(1-)*11H₂O=DyI(OH)2(H₂O)11

: 493-77-6
2,4,6-triphenyl-1,3,5-triazine

: 642-04-6
2,3,5,6-tetraphenylpyrazine

Guidance literature:: In benzonitrile; byproducts: 2,4,5-triphenylimidazole; conventional Schlenk technique; PhCN added with stirring to DyI2; 5 min;concd.; crystd. for 24 h; THF added to mother liquor; 1 h; decanted; so lvent removed from soln.; MeOH added; pptd. (20°C, 24 h); MeOH removed from soln.; pptd. by H2O; crystals after crystn. sepd. by decantation, washed with PhCN, dried (DyI3(PhCN)4); ppt. of Dy-THF complex washed with cold THF, dried in vac.; ppt. after H2O addition sepd. by centrifuging, washed with ether, dried (DyI(OH)2(H2O)11); elem. anal.;
DOI:10.1023/B:RUCB.0000037850.09936.95

Reference yield: 91.3%

: 1004-22-4
phenylethynylsodium

: 279221-53-3
tris(tetrahydrofurane)triiodidodysprosium(III)

: 279221-48-6
tris(phenylethynyl)(tetrahydrofurane)dysprosium(III)

Guidance literature:: In tetrahydrofuran; byproducts: NaI; suspension of ethynyl compd. addn. to soln. of lanthanide compd., stirring; solvent removing, residue treating with benzene, extracts combining, drying; elem. anal., IR spectroscopy;