((1S,6S)-6-((tert-butyldimethylsilyloxy)methyl)cyclohex-3-enyl)methyl iodide

Base Information

Chemical Name:((1S,6S)-6-((tert-butyldimethylsilyloxy)methyl)cyclohex-3-enyl)methyl iodide
CAS No.:956005-64-4
Molecular Formula:C₁₄H₂₇IOSi
Molecular Weight:366.358
Hs Code.:

Synonyms:((1S,6S)-6-((tert-butyldimethylsilyloxy)methyl)cyclohex-3-enyl)methyl iodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((1S,6S)-6-((tert-butyldimethylsilyloxy)methyl)cyclohex-3-enyl)methyl iodide

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Technology Process of ((1S,6S)-6-((tert-butyldimethylsilyloxy)methyl)cyclohex-3-enyl)methyl iodide

There total 2 articles about ((1S,6S)-6-((tert-butyldimethylsilyloxy)methyl)cyclohex-3-enyl)methyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 956005-60-0
((1S,6S)-6-((tert-butyldimethylsilyloxy)methyl)cyclohex-3-enyl)methanol

: 956005-64-4
((1S,6S)-6-((tert-butyldimethylsilyloxy)methyl)cyclohex-3-enyl)methyl iodide

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In dichloromethane; for 0.416667h;
DOI:10.1021/ol7017938

Reference yield:

: 15679-27-3
(4S,5S)-4,5-bis(hydroxymethyl)cyclohexene

: 956005-64-4
((1S,6S)-6-((tert-butyldimethylsilyloxy)methyl)cyclohex-3-enyl)methyl iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / n-BuLi / tetrahydrofuran; hexane / 20 °C

2: 81 percent / imidazole; PPh₃; I₂ / CH₂Cl₂ / 0.42 h

With 1H-imidazole; n-butyllithium; iodine; triphenylphosphine; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol7017938