N¹-(4-(4-(4-(dibutylamino)styryl)-2,3,5,6-tetrafluorostyryl)phenyl)-N¹-methylpropane-1,3-diamine

Base Information

• Chemical Name: N¹-(4-(4-(4-(dibutylamino)styryl)-2,3,5,6-tetrafluorostyryl)phenyl)-N¹-methylpropane-1,3-diamine
• CAS No.: 1426399-76-9
• Molecular Formula: C₃₄H₄₁F₄N₃
• Molecular Weight: 567.713

Synonyms:N¹-(4-(4-(4-(dibutylamino)styryl)-2,3,5,6-tetrafluorostyryl)phenyl)-N¹-methylpropane-1,3-diamine

Chemical Property of N¹-(4-(4-(4-(dibutylamino)styryl)-2,3,5,6-tetrafluorostyryl)phenyl)-N¹-methylpropane-1,3-diamine

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of N¹-(4-(4-(4-(dibutylamino)styryl)-2,3,5,6-tetrafluorostyryl)phenyl)-N¹-methylpropane-1,3-diamine

There total 8 articles about N¹-(4-(4-(4-(dibutylamino)styryl)-2,3,5,6-tetrafluorostyryl)phenyl)-N¹-methylpropane-1,3-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(E,E)-1-(4(dibutylamino)styryl)-4-(((3-(1,3-dioxoisoindolin-2-yl)propyl)(methyl)amino)styryl)-2,3,5,6-tetrafluorobenzene (1426399-75-8) → N1-(4-(4-(4-(dibutylamino)styryl)-2,3,5,6-tetrafluorostyryl)phenyl)-N1-methylpropane-1,3-diamine (1426399-76-9)

Guidance literature:

With hydrazine hydrate; In ethanol; Reflux;

DOI:10.1016/j.tet.2013.01.075

Reference yield:

[4-((diethoxyphosphoryl)methyl)-2,3,5,6-tetrafluorobenzyl]phosphonic acid diethyl ester (288627-04-3) → N1-(4-(4-(4-(dibutylamino)styryl)-2,3,5,6-tetrafluorostyryl)phenyl)-N1-methylpropane-1,3-diamine (1426399-76-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere

2.2: 3 h / 5 °C

3.1: hydrazine hydrate / ethanol / Reflux

With potassium tert-butylate; hydrazine hydrate; In tetrahydrofuran; ethanol; 1.1: |Horner-Wadsworth-Emmons Olefination / 1.2: |Horner-Wadsworth-Emmons Olefination / 2.2: |Horner-Wadsworth-Emmons Olefination;

DOI:10.1016/j.tet.2013.01.075

Reference yield:

N-methylaniline (100-61-8) → N1-(4-(4-(4-(dibutylamino)styryl)-2,3,5,6-tetrafluorostyryl)phenyl)-N1-methylpropane-1,3-diamine (1426399-76-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: potassium carbonate / acetonitrile / 18 h / Reflux

2.1: trichlorophosphate / 2.5 h / 0 - 20 °C / Inert atmosphere

2.2: 4 h / 95 °C / Inert atmosphere

3.1: potassium tert-butylate / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere

3.2: 3 h / 5 °C

4.1: hydrazine hydrate / ethanol / Reflux

With potassium tert-butylate; potassium carbonate; hydrazine hydrate; trichlorophosphate; In tetrahydrofuran; ethanol; acetonitrile; 3.2: |Horner-Wadsworth-Emmons Olefination;

DOI:10.1016/j.tet.2013.01.075

upstream raw materials:

α,α’-dibromo-m-tetrafluoroxylene

[4-((diethoxyphosphoryl)methyl)-2,3,5,6-tetrafluorobenzyl]phosphonic acid diethyl ester

(E)-diethyl 4-(4-(dibutylamino)styryl)-2,3,5,6-tetrafluorobenzylphosphonate

N-methylaniline

Downstream raw materials:

N-(3-((4-(4-(4-(dibutylamino)styryl)-2,3,5,6-tetrafluorostyryl)phenyl)(methyl)amino)propyl)acetamide

N¹-(3-((4-(4-(4-(dibutylamino)styryl)-2,3,5,6-tetrafluorostyryl)phenyl)(methyl)amino)propyl)-N³,N⁵-bis(3-(4-methyl-2-oxo-2H-chromen-7-yloxy)propyl)benzene-1,3,5-tricarboxamide

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