(E,E)-1-(4(dibutylamino)styryl)-4-(((3-(1,3-dioxoisoindolin-2-yl)propyl)(methyl)amino)styryl)-2,3,5,6-tetrafluorobenzene

Base Information

Chemical Name:(E,E)-1-(4(dibutylamino)styryl)-4-(((3-(1,3-dioxoisoindolin-2-yl)propyl)(methyl)amino)styryl)-2,3,5,6-tetrafluorobenzene
CAS No.:1426399-75-8
Molecular Formula:C₄₂H₄₃F₄N₃O₂
Molecular Weight:697.816
Hs Code.:

Synonyms:(E,E)-1-(4(dibutylamino)styryl)-4-(((3-(1,3-dioxoisoindolin-2-yl)propyl)(methyl)amino)styryl)-2,3,5,6-tetrafluorobenzene

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Chemical Property of (E,E)-1-(4(dibutylamino)styryl)-4-(((3-(1,3-dioxoisoindolin-2-yl)propyl)(methyl)amino)styryl)-2,3,5,6-tetrafluorobenzene

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Technology Process of (E,E)-1-(4(dibutylamino)styryl)-4-(((3-(1,3-dioxoisoindolin-2-yl)propyl)(methyl)amino)styryl)-2,3,5,6-tetrafluorobenzene

There total 7 articles about (E,E)-1-(4(dibutylamino)styryl)-4-(((3-(1,3-dioxoisoindolin-2-yl)propyl)(methyl)amino)styryl)-2,3,5,6-tetrafluorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1426399-73-6
(E)-diethyl 4-(4-(dibutylamino)styryl)-2,3,5,6-tetrafluorobenzylphosphonate

: 1426399-74-7
4-((3-(1,3-dioxoisoindolin-2-yl)propyl)(methyl)amino)benzaldehyde

: 1426399-75-8
(E,E)-1-(4(dibutylamino)styryl)-4-(((3-(1,3-dioxoisoindolin-2-yl)propyl)(methyl)amino)styryl)-2,3,5,6-tetrafluorobenzene

Guidance literature:: (E)-diethyl 4-(4-(dibutylamino)styryl)-2,3,5,6-tetrafluorobenzylphosphonate; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.0833333h; Inert atmosphere;

4-((3-(1,3-dioxoisoindolin-2-yl)propyl)(methyl)amino)benzaldehyde; In tetrahydrofuran; at 5 ℃; for 3h;
DOI:10.1016/j.tet.2013.01.075

Reference yield:

: 288627-04-3
[4-((diethoxyphosphoryl)methyl)-2,3,5,6-tetrafluorobenzyl]phosphonic acid diethyl ester

: 1426399-75-8
(E,E)-1-(4(dibutylamino)styryl)-4-(((3-(1,3-dioxoisoindolin-2-yl)propyl)(methyl)amino)styryl)-2,3,5,6-tetrafluorobenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere

2.2: 3 h / 5 °C

With potassium tert-butylate; In tetrahydrofuran; 1.1: |Horner-Wadsworth-Emmons Olefination / 1.2: |Horner-Wadsworth-Emmons Olefination / 2.2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1016/j.tet.2013.01.075

Reference yield:

: 100-61-8
N-methylaniline

: 1426399-75-8
(E,E)-1-(4(dibutylamino)styryl)-4-(((3-(1,3-dioxoisoindolin-2-yl)propyl)(methyl)amino)styryl)-2,3,5,6-tetrafluorobenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetonitrile / 18 h / Reflux

2.1: trichlorophosphate / 2.5 h / 0 - 20 °C / Inert atmosphere

2.2: 4 h / 95 °C / Inert atmosphere

3.1: potassium tert-butylate / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere

3.2: 3 h / 5 °C

With potassium tert-butylate; potassium carbonate; trichlorophosphate; In tetrahydrofuran; acetonitrile; 3.2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1016/j.tet.2013.01.075