C₄₅H₅₉BrO₁₄

Base Information

Chemical Name:C₄₅H₅₉BrO₁₄
CAS No.:328084-38-4
Molecular Formula:C₄₅H₅₉BrO₁₄
Molecular Weight:903.859
Hs Code.:

C<sub>45</sub>H<sub>59</sub>BrO<sub>14</sub>

Synonyms:C₄₅H₅₉BrO₁₄

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Chemical Property of C₄₅H₅₉BrO₁₄

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Technology Process of C₄₅H₅₉BrO₁₄

There total 5 articles about C₄₅H₅₉BrO₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 328084-37-3
C₄₅H₆₀O₁₅

: 328084-38-4
C₄₅H₅₉BrO₁₄

Guidance literature:: With carbon tetrabromide; triphenylphosphine; Inert atmosphere;
DOI:10.1039/b815263b

Reference yield:

: 29654-55-5
5-(hydroxymethyl)benzene-1,3-diol

: 328084-38-4
C₄₅H₅₉BrO₁₄

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; 18-crown-6 ether / acetone / 36 h / Reflux

2: triphenylphosphine; carbon tetrabromide / dichloromethane / 0.17 h / 20 °C

With 18-crown-6 ether; carbon tetrabromide; potassium carbonate; triphenylphosphine; In dichloromethane; acetone;
DOI:10.1021/acs.joc.1c00195

Reference yield:

: 99-10-5
3,5-Dihydroxybenzoic acid

: 328084-38-4
C₄₅H₅₉BrO₁₄

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylsulfide borane complex; Trimethyl borate / tetrahydrofuran / 24 h / Reflux

2: potassium carbonate; 18-crown-6 ether / acetone / 36 h / Reflux

3: triphenylphosphine; carbon tetrabromide / dichloromethane / 0.17 h / 20 °C

With 18-crown-6 ether; Trimethyl borate; carbon tetrabromide; dimethylsulfide borane complex; potassium carbonate; triphenylphosphine; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/acs.joc.1c00195