benzhydryl 2β-(chloroacetoxy)methyl-1,1-dioxo-penicillanate

Base Information

Chemical Name:benzhydryl 2β-(chloroacetoxy)methyl-1,1-dioxo-penicillanate
CAS No.:182750-64-7
Molecular Formula:C₂₃H₂₂ClNO₇S
Molecular Weight:491.949
Hs Code.:

Synonyms:benzhydryl 2β-(chloroacetoxy)methyl-1,1-dioxo-penicillanate

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Chemical Property of benzhydryl 2β-(chloroacetoxy)methyl-1,1-dioxo-penicillanate

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Technology Process of benzhydryl 2β-(chloroacetoxy)methyl-1,1-dioxo-penicillanate

There total 5 articles about benzhydryl 2β-(chloroacetoxy)methyl-1,1-dioxo-penicillanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: benzhydryl 2β-(chloroacetoxy)methyl-penicillanate

: 182750-64-7
benzhydryl 2β-(chloroacetoxy)methyl-1,1-dioxo-penicillanate

Guidance literature:: With potassium permanganate; acetic acid; In water; acetone; at 20 ℃; for 1h;
DOI:10.1128/AAC.06099-11

Reference yield:

: 2-[2-(1H-inden-2-yldisulfanyl)-4-oxo-azetidin-1-yl]-3-methyl-but-3-enoic acid benzhydryl ester

: 79-11-8
chloroacetic acid

: (R)-3-(2-Chloro-acetoxy)-3-methyl-5,5,8-trioxo-5λ⁶-thia-1-aza-bicyclo[4.2.0]octane-2-carboxylic acid benzhydryl ester

: 182750-64-7
benzhydryl 2β-(chloroacetoxy)methyl-1,1-dioxo-penicillanate

Guidance literature:: 2-[2-(1H-inden-2-yldisulfanyl)-4-oxo-azetidin-1-yl]-3-methyl-but-3-enoic acid benzhydryl ester; chloroacetic acid; With silver(I) acetate;

With potassium permanganate; acetic acid; In acetone;
DOI:10.1016/j.bmc.2005.02.020

Reference yield:

: 551-16-6
6-Aminopenicillanic Acid

: 182750-64-7
benzhydryl 2β-(chloroacetoxy)methyl-1,1-dioxo-penicillanate

Guidance literature:: Multi-step reaction with 6 steps

1: sulfuric acid; potassium bromide; sodium nitrite / ethanol / 3.5 h / 6 - 8 °C

2: peracetic acid; potassium iodide / dichloromethane; water / 1 h / 0 °C

3: acetic acid; zinc / acetonitrile / 1 h / 0 °C

4: toluene / 2 h / 114 °C

5: silver(I) acetate / dichloromethane / 4 h / 20 °C

6: potassium permanganate; acetic acid / water; acetone / 1 h / 20 °C

With peracetic acid; potassium permanganate; sulfuric acid; silver(I) acetate; acetic acid; potassium iodide; potassium bromide; zinc; sodium nitrite; In ethanol; dichloromethane; water; acetone; toluene; acetonitrile;
DOI:10.1128/AAC.06099-11