-p-nitrobenzoic acid

Base Information

Chemical Name:-p-nitrobenzoic acid
CAS No.:69838-88-6
Molecular Formula:C₇H₅NO₄
Molecular Weight:168.11
Hs Code.:

Synonyms:-p-nitrobenzoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of -p-nitrobenzoic acid

Chemical Property:

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Technology Process of -p-nitrobenzoic acid

There total 6 articles about -p-nitrobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.4%

: 74568-18-6
-p-aminobenzoic acid

: 69838-88-6
-p-nitrobenzoic acid

Guidance literature:: With sulfuric acid; dihydrogen peroxide; trifluoroacetic acid; at 73 - 76 ℃; 2 h; 2 h;
DOI:10.1002/poc.610070504

Reference yield: 65.0%

: 1111-72-4
carbon dioxide

: 81456-99-7
4-nitrobenzoic acid cesium salt

: 69838-88-6
-p-nitrobenzoic acid

Guidance literature:: With 2,2-bis((S)-4-phenyl-4,5-dihydrooxazol-2-yl)acetonitrile; copper(I) bromide; In dimethyl sulfoxide; at 150 ℃; for 2h; chemoselective reaction; Inert atmosphere; Glovebox; Cooling with liquid nitrogen;
DOI:10.1021/jacs.8b12140

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 69838-88-6
-p-nitrobenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: bis(tri-t-butylphosphine)palladium⁽⁰⁾ / toluene / 75 °C / Sealed tube

2: water / toluene / 2 h / Sealed tube

With bis(tri-t-butylphosphine)palladium⁽⁰⁾; water; In toluene;
DOI:10.1021/jacs.8b09808