2-[2-[2-[4-[tris[4-(tert-butyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethanol

Base Information

• Chemical Name: 2-[2-[2-[4-[tris[4-(tert-butyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethanol
• CAS No.: 351523-94-9
• Molecular Formula: C₄₃H₅₆O₄
• Molecular Weight: 636.915
• Mol file: 351523-94-9.mol

Synonyms:2-[2-[2-[4-[tris[4-(tert-butyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethanol

Chemical Property of 2-[2-[2-[4-[tris[4-(tert-butyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-[2-[2-[4-[tris[4-(tert-butyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethanol

There total 2 articles about 2-[2-[2-[4-[tris[4-(tert-butyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-[2-(chloroethoxy)ethoxy]ethanol (5197-62-6) + 4-[tris-(4-tert-butylphenyl)methyl]phenol (143998-20-3) → 2-[2-[2-[4-[tris[4-(tert-butyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethanol (351523-94-9)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 48h;

DOI:10.1002/chem.200802510

Reference yield: 75.0%

4-[tris-(4-tert-butylphenyl)methyl]phenol (143998-20-3) + 2,2'-[1,2-ethanediylbis(oxy)]bisethanol (112-27-6) → 2-[2-[2-[4-[tris[4-(tert-butyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethanol (351523-94-9)

Guidance literature:

4-[tris-(4-tert-butylphenyl)methyl]phenol; With potassium hydroxide; In water; butan-1-ol; for 0.25h; Reflux; Inert atmosphere;

2,2'-[1,2-ethanediylbis(oxy)]bisethanol; In water; butan-1-ol; for 72h; Reflux; Inert atmosphere;

DOI:10.1021/ja5013596

Reference yield: 99.0%

2-[2-[2-[4-[tris[4-(tert-butyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethanol (351523-94-9) → 2-[2-(2-{4-[tris(4-t-butylphenyl)methyl]phenoxy}ethoxy)ethoxy]ethyl bromide (1596368-20-5)

Guidance literature:

With carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 49h; Inert atmosphere;

DOI:10.1021/ja5013596

upstream raw materials:

2-[2-(chloroethoxy)ethoxy]ethanol

4-[tris-(4-tert-butylphenyl)methyl]phenol

2,2'-[1,2-ethanediylbis(oxy)]bisethanol

Downstream raw materials:

C₄₄H₅₈O₆S

((CH₃)3CC₆H₄)3CC₆H₄O(CH₂CH₂O)3C₆H₄C₁₂H₆N₂C₆H₄Br

((CH₃)3CC₆H₄)3CC₆H₄O(CH₂CH₂O)3C₆H₄C₁₂H₆N₂C₆H₄B(neopentyl glycolato)

2-(2-(2-[4-(tris(4-tert-butylphenyl)methyl)phenoxy]ethoxy)ethoxy)ethyl iodide