2-[2-(2-{4-[tris(4-t-butylphenyl)methyl]phenoxy}ethoxy)ethoxy]ethyl bromide

Base Information

Chemical Name:2-[2-(2-{4-[tris(4-t-butylphenyl)methyl]phenoxy}ethoxy)ethoxy]ethyl bromide
CAS No.:1596368-20-5
Molecular Formula:C₄₃H₅₅BrO₃
Molecular Weight:699.812
Hs Code.:

Synonyms:2-[2-(2-{4-[tris(4-t-butylphenyl)methyl]phenoxy}ethoxy)ethoxy]ethyl bromide

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Chemical Property of 2-[2-(2-{4-[tris(4-t-butylphenyl)methyl]phenoxy}ethoxy)ethoxy]ethyl bromide

Chemical Property:

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Technology Process of 2-[2-(2-{4-[tris(4-t-butylphenyl)methyl]phenoxy}ethoxy)ethoxy]ethyl bromide

There total 3 articles about 2-[2-(2-{4-[tris(4-t-butylphenyl)methyl]phenoxy}ethoxy)ethoxy]ethyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 351523-94-9
2-[2-[2-[4-[tris[4-(tert-butyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethanol

: 1596368-20-5
2-[2-(2-{4-[tris(4-t-butylphenyl)methyl]phenoxy}ethoxy)ethoxy]ethyl bromide

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 49h; Inert atmosphere;
DOI:10.1021/ja5013596

Reference yield:

: 143998-20-3
4-[tris-(4-tert-butylphenyl)methyl]phenol

: 1596368-20-5
2-[2-(2-{4-[tris(4-t-butylphenyl)methyl]phenoxy}ethoxy)ethoxy]ethyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / butan-1-ol; water / 0.25 h / Reflux; Inert atmosphere

1.2: 72 h / Reflux; Inert atmosphere

2.1: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 49 h / 0 - 20 °C / Inert atmosphere

With carbon tetrabromide; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; water; butan-1-ol;
DOI:10.1021/ja5013596

Reference yield:

: 112-27-6
2,2'-[1,2-ethanediylbis(oxy)]bisethanol

: 1596368-20-5
2-[2-(2-{4-[tris(4-t-butylphenyl)methyl]phenoxy}ethoxy)ethoxy]ethyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / butan-1-ol; water / 0.25 h / Reflux; Inert atmosphere

1.2: 72 h / Reflux; Inert atmosphere

2.1: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 49 h / 0 - 20 °C / Inert atmosphere

With carbon tetrabromide; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; water; butan-1-ol;
DOI:10.1021/ja5013596