(1S,2R,3R)-1-(2,6-diiodo-3,5-dimethoxyphenoxy)-1-(4-methoxyphenyl)-3-trimethylsilyl-2,3-epoxypropane

Base Information

Chemical Name:(1S,2R,3R)-1-(2,6-diiodo-3,5-dimethoxyphenoxy)-1-(4-methoxyphenyl)-3-trimethylsilyl-2,3-epoxypropane
CAS No.:147622-57-9
Molecular Formula:C₂₁H₂₆I₂O₅Si
Molecular Weight:640.329
Hs Code.:

Synonyms:(1S,2R,3R)-1-(2,6-diiodo-3,5-dimethoxyphenoxy)-1-(4-methoxyphenyl)-3-trimethylsilyl-2,3-epoxypropane

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Chemical Property of (1S,2R,3R)-1-(2,6-diiodo-3,5-dimethoxyphenoxy)-1-(4-methoxyphenyl)-3-trimethylsilyl-2,3-epoxypropane

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Technology Process of (1S,2R,3R)-1-(2,6-diiodo-3,5-dimethoxyphenoxy)-1-(4-methoxyphenyl)-3-trimethylsilyl-2,3-epoxypropane

There total 1 articles about (1S,2R,3R)-1-(2,6-diiodo-3,5-dimethoxyphenoxy)-1-(4-methoxyphenyl)-3-trimethylsilyl-2,3-epoxypropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 147622-60-4
2,6-diiodo-3,5-dimethyoxyphenol

: 147622-51-3
(R)-(4-Methoxy-phenyl)-((2R,3R)-3-trimethylsilanyl-oxiranyl)-methanol

: 147650-56-4
(1R,2R,3R)-1-(2,6-diiodo-3,5-dimethoxyphenoxy)-1-(4-methoxyphenyl)-3-trimethylsilyl-2,3-epoxypropane

: 147622-57-9
(1S,2R,3R)-1-(2,6-diiodo-3,5-dimethoxyphenoxy)-1-(4-methoxyphenyl)-3-trimethylsilyl-2,3-epoxypropane

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; Title compound not separated from byproducts; Ambient temperature;
DOI:10.1016/S0040-4020(01)80702-X

Reference yield: 99.0%

: 147622-57-9
(1S,2R,3R)-1-(2,6-diiodo-3,5-dimethoxyphenoxy)-1-(4-methoxyphenyl)-3-trimethylsilyl-2,3-epoxypropane

: (1R,2S)-1-(2,6-diiodo-3,5-dimethoxyphenoxy)-1-(4-methoxyphenyl)-2,3-epoxypropane

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)80702-X

Reference yield:

: 147622-57-9
(1S,2R,3R)-1-(2,6-diiodo-3,5-dimethoxyphenoxy)-1-(4-methoxyphenyl)-3-trimethylsilyl-2,3-epoxypropane

: 3-(3,5-dimethoxyphenoxy)-3-(4-methoxyphenyl)prop-2-en-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / 1 M tetrabutylammonium fluoride / tetrahydrofuran

2: 75 percent / n-BuLi, MgBr₂ / tetrahydrofuran; hexane

With n-butyllithium; tetrabutyl ammonium fluoride; magnesium bromide; In tetrahydrofuran; hexane;
DOI:10.1016/S0040-4020(01)80702-X