5-O-allyl-1,2,3-tri-O-benzyl-4-O-(2,3-di-O-acetyl-4,6-O-ethylidene-β-D-glucopyranosyl)-D-ribitol

Base Information

Chemical Name:5-O-allyl-1,2,3-tri-O-benzyl-4-O-(2,3-di-O-acetyl-4,6-O-ethylidene-β-D-glucopyranosyl)-D-ribitol
CAS No.:116490-78-9
Molecular Formula:C₄₁H₅₀O₁₂
Molecular Weight:734.841
Hs Code.:

Synonyms:5-O-allyl-1,2,3-tri-O-benzyl-4-O-(2,3-di-O-acetyl-4,6-O-ethylidene-β-D-glucopyranosyl)-D-ribitol

Suppliers and Price of 5-O-allyl-1,2,3-tri-O-benzyl-4-O-(2,3-di-O-acetyl-4,6-O-ethylidene-β-D-glucopyranosyl)-D-ribitol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-O-allyl-1,2,3-tri-O-benzyl-4-O-(2,3-di-O-acetyl-4,6-O-ethylidene-β-D-glucopyranosyl)-D-ribitol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 5-O-allyl-1,2,3-tri-O-benzyl-4-O-(2,3-di-O-acetyl-4,6-O-ethylidene-β-D-glucopyranosyl)-D-ribitol

There total 2 articles about 5-O-allyl-1,2,3-tri-O-benzyl-4-O-(2,3-di-O-acetyl-4,6-O-ethylidene-β-D-glucopyranosyl)-D-ribitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 116490-77-8
2,3-di-O-acetyl-4,6-O-ethylidene-α-D-glucopyranosyl bromide

: 116490-76-7
5-O-allyl-1,2,3-tri-O-benzyl-D-ribitol

: 116524-94-8
3-O-acetyl-1,2-cyanoethylidene-4,6-O-ethylidene-α-D-glucopyranose

: 116490-78-9
5-O-allyl-1,2,3-tri-O-benzyl-4-O-(2,3-di-O-acetyl-4,6-O-ethylidene-β-D-glucopyranosyl)-D-ribitol

Guidance literature:: With 3 A molecular sieve; mercury(II) cyanide; mercury dibromide; In nitromethane; benzene;
DOI:10.1016/0008-6215(88)84144-2

Reference yield:

: 29810-01-3
1,2,3-tri-O-acetyl-4,6-O-ethylidene-α-D-glucopyranose

: 116490-78-9
5-O-allyl-1,2,3-tri-O-benzyl-4-O-(2,3-di-O-acetyl-4,6-O-ethylidene-β-D-glucopyranosyl)-D-ribitol

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen bromide / CH₂Cl₂ / 2 h / -20 °C

2: 86 percent / mercuric bromode, mercuric cyanide, pulverised molecular sieves (3 A) / benzene; nitromethane

With 3 A molecular sieve; hydrogen bromide; mercury(II) cyanide; mercury dibromide; In nitromethane; dichloromethane; benzene;
DOI:10.1016/0008-6215(88)84144-2