1,3-dimethyl-2,4,6-trioxo-hexahydro-pyrimidine-5-carboxylic acid 4-chloro-anilide

Base Information

• Chemical Name: 1,3-dimethyl-2,4,6-trioxo-hexahydro-pyrimidine-5-carboxylic acid 4-chloro-anilide
• CAS No.: 65400-89-7
• Molecular Formula: C₁₃H₁₂ClN₃O₄
• Molecular Weight: 309.709

Synonyms:1,3-dimethyl-2,4,6-trioxo-hexahydro-pyrimidine-5-carboxylic acid 4-chloro-anilide

Chemical Property of 1,3-dimethyl-2,4,6-trioxo-hexahydro-pyrimidine-5-carboxylic acid 4-chloro-anilide

Chemical Property:

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Technology Process of 1,3-dimethyl-2,4,6-trioxo-hexahydro-pyrimidine-5-carboxylic acid 4-chloro-anilide

There total 3 articles about 1,3-dimethyl-2,4,6-trioxo-hexahydro-pyrimidine-5-carboxylic acid 4-chloro-anilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1,3-dimethylbarbituric acid (769-42-6) + phenyl N-(4-chlorophenyl)carbamate (50882-28-5) → 1,3-dimethyl-2,4,6-trioxo-hexahydro-pyrimidine-5-carboxylic acid 4-chloro-anilide (65400-89-7)

Guidance literature:

1,3-dimethylbarbituric acid; With sodium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 1h; Sonication;

phenyl N-(4-chlorophenyl)carbamate; In N,N-dimethyl-formamide; at 100 - 130 ℃; for 4h; Sonication;

DOI:10.1016/j.bmc.2016.09.074

Reference yield:

1,3-dimethylbarbituric acid (769-42-6) + p-chlorphenylisocyanate (104-12-1) → 1,3-dimethyl-2,4,6-trioxo-hexahydro-pyrimidine-5-carboxylic acid 4-chloro-anilide (65400-89-7)

Guidance literature:

With hydrogenchloride; triethylamine; In water; dimethyl sulfoxide;

Reference yield:

→ 1,3-dimethyl-2,4,6-trioxo-hexahydro-pyrimidine-5-carboxylic acid 4-chloro-anilide (65400-89-7)

Guidance literature:

entspr. Barbitursaeure, Isocyanat;

upstream raw materials:

1,3-dimethylbarbituric acid

p-chlorphenylisocyanate

phenyl N-(4-chlorophenyl)carbamate

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