PHENYL N-(4-CHLOROPHENYL)CARBAMATE

Base Information

• Chemical Name: PHENYL N-(4-CHLOROPHENYL)CARBAMATE
• CAS No.: 50882-28-5
• Molecular Formula: C13H10 Cl N O2
• Molecular Weight: 247.681
• Hs Code.: 2924299090
• Mol file: 50882-28-5.mol

Synonyms:Carbamicacid, (4-chlorophenyl)-, phenyl ester (9CI); Phenyl (4-chlorophenyl)carbamate;Phenyl N-(4-chlorophenyl)carbamate; Phenyl p-chlorocarbanilate

Chemical Property of PHENYL N-(4-CHLOROPHENYL)CARBAMATE

Chemical Property:

• Vapor Pressure: 6.85E-05mmHg at 25°C
• Melting Point: 185 °C
• Boiling Point: 343.8°Cat760mmHg
• PKA: 12.15±0.70(Predicted)
• Flash Point: 161.7°C
• PSA: 38.33000
• Density: 1.329g/cm³
• LogP: 4.02390

Purity/Quality:

99% ^*data from raw suppliers

PHENYL N-(4-CHLOROPHENYL)CARBAMATE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of PHENYL N-(4-CHLOROPHENYL)CARBAMATE

There total 6 articles about PHENYL N-(4-CHLOROPHENYL)CARBAMATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.2%

4-chloro-aniline (106-47-8) + phenyl chloroformate (1885-14-9) → phenyl N-(4-chlorophenyl)carbamate (50882-28-5)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 20 ℃; for 3h;

DOI:10.1016/j.bioorg.2014.07.011

Reference yield: 93.0%

p-chlorphenylisocyanate (104-12-1) + phenol (108-95-2,27073-41-2) → phenyl N-(4-chlorophenyl)carbamate (50882-28-5)

Guidance literature:

In toluene; at 110 ℃; for 3h; Inert atmosphere;

Reference yield: 90.0%

phenyl 4,5-dichloro-6-oxopyridazine-1(6H)-carboxylate (1202680-24-7) + 4-chloro-aniline (106-47-8) → phenyl N-(4-chlorophenyl)carbamate (50882-28-5)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 0.666667h;

DOI:10.1055/s-0029-1217997

upstream raw materials:

4-chlorobenzoyl azide

phenol

4-chloro-aniline

phenyl chloroformate

Downstream raw materials:

N-butyl-4-chlorobenzamide

phenol

3-(4-chlorophenyl)-1-(4-tolyl)urea

p-chlorophenylsemicarbazide