2,4-difluoro-6-(5-(thiophen-3-yl)-1H-pyrrolo[2,3-b]pyridin-3-yl)phenol

Base Information

Chemical Name:2,4-difluoro-6-(5-(thiophen-3-yl)-1H-pyrrolo[2,3-b]pyridin-3-yl)phenol
CAS No.:1613710-38-5
Molecular Formula:C₁₇H₁₀F₂N₂OS
Molecular Weight:328.342
Hs Code.:

Synonyms:2,4-difluoro-6-(5-(thiophen-3-yl)-1H-pyrrolo[2,3-b]pyridin-3-yl)phenol

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Chemical Property of 2,4-difluoro-6-(5-(thiophen-3-yl)-1H-pyrrolo[2,3-b]pyridin-3-yl)phenol

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Technology Process of 2,4-difluoro-6-(5-(thiophen-3-yl)-1H-pyrrolo[2,3-b]pyridin-3-yl)phenol

There total 4 articles about 2,4-difluoro-6-(5-(thiophen-3-yl)-1H-pyrrolo[2,3-b]pyridin-3-yl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1613712-45-0
C₂₄H₁₆F₂N₂O₃S₂

: 1613710-38-5
2,4-difluoro-6-(5-(thiophen-3-yl)-1H-pyrrolo[2,3-b]pyridin-3-yl)phenol

Guidance literature:: With water; potassium carbonate; In methanol; at 30 ℃; for 12h;

Reference yield:

: 875639-15-9
5-bromo-3-iodo-1-(4-methylbenzene-1-sulfonyl)-1H-pyrrolo[2,3-b]pyridine

: 1613710-38-5
2,4-difluoro-6-(5-(thiophen-3-yl)-1H-pyrrolo[2,3-b]pyridin-3-yl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / acetonitrile / 4 h / 90 °C

2: caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile / 12 h / 90 °C

3: potassium carbonate; water / methanol / 12 h / 30 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; water; potassium carbonate; caesium carbonate; In methanol; acetonitrile;

Reference yield:

: 1613712-44-9
C₂₀H₁₃BrF₂N₂O₃S

: 1613710-38-5
2,4-difluoro-6-(5-(thiophen-3-yl)-1H-pyrrolo[2,3-b]pyridin-3-yl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile / 12 h / 90 °C

2: potassium carbonate; water / methanol / 12 h / 30 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; potassium carbonate; caesium carbonate; In methanol; acetonitrile;