Technology Process of N-1-benzyl-4-tert-butylbenzene-1,2-diamine
There total 6 articles about N-1-benzyl-4-tert-butylbenzene-1,2-diamine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
benzyl-(4-tert-butyl-2-nitrophenyl)amine;
In
methanol;
for 0.166667h;
Large scale;
With
hydrogen;
In
methanol;
at 20 ℃;
for 10h;
Large scale;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium hydroxide / toluene; dimethyl sulfoxide / 0.67 h / 20 °C / Large scale
1.2: 4 h / 10 °C / Large scale
2.1: methanol / 0.17 h / Large scale
2.2: Raney nickel / 10 h / 20 °C / Large scale
With
potassium hydroxide;
In
methanol; dimethyl sulfoxide; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetic acid; acetic anhydride / 0.42 h / 20 °C / Large scale
1.2: 2 h / 20 - 25 °C / Large scale
2.1: methanol; sodium methylate / 2 h / 20 °C / Reflux; Large scale
3.1: potassium hydroxide / toluene; dimethyl sulfoxide / 0.67 h / 20 °C / Large scale
3.2: 4 h / 10 °C / Large scale
4.1: methanol / 0.17 h / Large scale
4.2: Raney nickel / 10 h / 20 °C / Large scale
With
methanol; sodium methylate; acetic anhydride; acetic acid; potassium hydroxide;
In
methanol; dimethyl sulfoxide; toluene;
