N-glycine ethyl ester

Base Information

Chemical Name:N-glycine ethyl ester
CAS No.:103112-01-2
Molecular Formula:C₁₂H₁₅NO₂S
Molecular Weight:237.323
Hs Code.:

N-<methylthio(phenyl)methylene>glycine ethyl ester

Synonyms:N-glycine ethyl ester

Suppliers and Price of N-glycine ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-glycine ethyl ester

Chemical Property:

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Technology Process of N-glycine ethyl ester

There total 3 articles about N-glycine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 87386-07-0
N-(thiobenzoyl)glycine ethyl ester

: 420-37-1
trimethoxonium tetrafluoroborate

: 103112-01-2
N-glycine ethyl ester

Guidance literature:: In dichloromethane; at -78 - 0 ℃; for 2h;
DOI:10.1055/s-1994-25715 DOI:10.1246/bcsj.67.2219

Reference yield:

: 1499-53-2
ethyl hippurate

: 103112-01-2
N-glycine ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 99.7 percent / Lawesson's reagent / tetrahydrofuran / 0.5 h / Heating

2: 100 percent / CH₂Cl₂ / 2 h / -78 - 0 °C

With Lawessons reagent; In tetrahydrofuran; dichloromethane;
DOI:10.1246/bcsj.67.2219

Reference yield:

: 98-88-4
benzoyl chloride

: 103112-01-2
N-glycine ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 99.4 percent / triethylamine / CH₂Cl₂ / 1 h / 0 °C

2: 99.7 percent / Lawesson's reagent / tetrahydrofuran / 0.5 h / Heating

3: 100 percent / CH₂Cl₂ / 2 h / -78 - 0 °C

With Lawessons reagent; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1246/bcsj.67.2219