1-(1,1-dimethylethyl) 3-methyl 4-(4-chlorophenyl)-5,6-dihydro-1,3(2H)-pyridinedicarboxylate

Base Information

Chemical Name:1-(1,1-dimethylethyl) 3-methyl 4-(4-chlorophenyl)-5,6-dihydro-1,3(2H)-pyridinedicarboxylate
CAS No.:1013097-55-6
Molecular Formula:C₁₈H₂₂ClNO₄
Molecular Weight:351.83
Hs Code.:

Synonyms:1-(1,1-dimethylethyl) 3-methyl 4-(4-chlorophenyl)-5,6-dihydro-1,3(2H)-pyridinedicarboxylate

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Chemical Property of 1-(1,1-dimethylethyl) 3-methyl 4-(4-chlorophenyl)-5,6-dihydro-1,3(2H)-pyridinedicarboxylate

Chemical Property:

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Technology Process of 1-(1,1-dimethylethyl) 3-methyl 4-(4-chlorophenyl)-5,6-dihydro-1,3(2H)-pyridinedicarboxylate

There total 2 articles about 1-(1,1-dimethylethyl) 3-methyl 4-(4-chlorophenyl)-5,6-dihydro-1,3(2H)-pyridinedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1679-18-1
4-Chlorophenylboronic acid

: 161491-24-3
methyl 1-tert-butoxycarbonyl-4-oxo-3-piperidinecarboxylate

: 1013097-55-6
1-(1,1-dimethylethyl) 3-methyl 4-(4-chlorophenyl)-5,6-dihydro-1,3(2H)-pyridinedicarboxylate

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; at 80 ℃; for 2h;

Reference yield:

: 161491-25-4
1-tert-butyl 3-methyl 4-(((trifluoromethyl)sulfonyl)oxy)-5,6-dihydropyridine-1,3(2H)-dicarboxylate

: 1679-18-1
4-Chlorophenylboronic acid

: 1013097-55-6
1-(1,1-dimethylethyl) 3-methyl 4-(4-chlorophenyl)-5,6-dihydro-1,3(2H)-pyridinedicarboxylate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; toluene; at 80 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jm100481d

Reference yield:

: 1013097-55-6
1-(1,1-dimethylethyl) 3-methyl 4-(4-chlorophenyl)-5,6-dihydro-1,3(2H)-pyridinedicarboxylate

: 1013097-56-7
tert-butyl 4-(4-chlorophenyl)-5-(hydroxymethyl)-3,6-dihydropyridine-1(2H)-carboxylate

Guidance literature:: 1-(1,1-dimethylethyl) 3-methyl 4-(4-chlorophenyl)-5,6-dihydro-1,3(2H)-pyridinedicarboxylate; With lithium aluminium tetrahydride; In diethyl ether; at -20 ℃; for 0.333333h;

With hydrogenchloride; water; In diethyl ether;