ALPHA-AMINOBENZENEACETYL CHLORIDE

Base Information

• Chemical Name: ALPHA-AMINOBENZENEACETYL CHLORIDE
• CAS No.: 39478-47-2
• Molecular Formula: C8H8 Cl N O
• Molecular Weight: 169.611
• Hs Code.: 2922499990
• Mol file: 39478-47-2.mol

Synonyms:a-Aminophenylacetyl chloride

Chemical Property of ALPHA-AMINOBENZENEACETYL CHLORIDE

Chemical Property:

• Vapor Pressure: 0.026mmHg at 25°C
• Boiling Point: 247.2°Cat760mmHg
• PKA: 6.15±0.10(Predicted)
• Flash Point: 103.3°C
• PSA: 43.09000
• Density: 1.254g/cm³
• LogP: 2.15210

Purity/Quality:

99%, ^*data from raw suppliers

Amino(phenyl)acetylchloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ALPHA-AMINOBENZENEACETYL CHLORIDE

There total 1 articles about ALPHA-AMINOBENZENEACETYL CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylglycin (2835-06-5) → amino-phenyl-acetyl chloride (39478-47-2)

Guidance literature:

Reference yield:

methanol (67-56-1) + amino-phenyl-acetyl chloride (39478-47-2) → phenylglycine methyl ester (24461-61-8,26682-99-5,37760-98-8,6591-61-3)

Guidance literature:

With potassium carbonate; at 20 ℃; for 0.25h;

DOI:10.1039/b813007h

Reference yield:

amino-phenyl-acetyl chloride (39478-47-2) + diphenylmethyl 7β-amino-2-<(Z)-(methoxycarbonyl)methylene>-3-methyl-3-cephem-4-carboxylate p-toluenesulfonic acid salt (90913-29-4) → (6R,7R)-7-(2-Amino-2-phenyl-acetylamino)-4-[1-methoxycarbonyl-meth-(Z)-ylidene]-3-methyl-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid benzhydryl ester

Guidance literature:

With triethylamine; 2,3-Dimethylaniline; In dichloromethane; at 5 ℃; for 2h;

DOI:10.1021/jm00375a026

upstream raw materials:

phenylglycin

Downstream raw materials:

3-methoxymethyl-7-D-phenylglycylamino-3-cephem-4-carbonsaeure

3-Ethoxymethyl-7-D-phenylglycylamino-3-cephem-4-carbonsaeure

Potassium; (2S,5R,6S)-6-[3-(2-amino-2-phenyl-acetyl)-thioureido]-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

(6R,7R)-7-(2-Amino-2-phenyl-acetylamino)-4-[1-methoxycarbonyl-meth-(Z)-ylidene]-3-methyl-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid

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