3-(2-ethyl-1,3-dioxolan-2-yl)propyltriphenylphosphonium iodide

Base Information

Chemical Name:3-(2-ethyl-1,3-dioxolan-2-yl)propyltriphenylphosphonium iodide
CAS No.:96890-24-3
Molecular Formula:C₂₆H₃₀O₂P*I
Molecular Weight:532.401
Hs Code.:

Synonyms:3-(2-ethyl-1,3-dioxolan-2-yl)propyltriphenylphosphonium iodide

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Chemical Property of 3-(2-ethyl-1,3-dioxolan-2-yl)propyltriphenylphosphonium iodide

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Technology Process of 3-(2-ethyl-1,3-dioxolan-2-yl)propyltriphenylphosphonium iodide

There total 6 articles about 3-(2-ethyl-1,3-dioxolan-2-yl)propyltriphenylphosphonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 112776-53-1
(4-oxohexyl)triphenylphosphonium iodide

: 107-21-1
ethylene glycol

: 96890-24-3
3-(2-ethyl-1,3-dioxolan-2-yl)propyltriphenylphosphonium iodide

Guidance literature:: With 4 A molecular sieve; toluene-4-sulfonic acid; In chloroform; for 36h;
DOI:10.1016/S0040-4020(01)86399-7

Reference yield: 83.0%

: 96890-23-2
2-ethyl-2-(3-iodopropyl)-1,3-dioxolane

: 603-35-0
triphenylphosphine

: 96890-24-3
3-(2-ethyl-1,3-dioxolan-2-yl)propyltriphenylphosphonium iodide

Guidance literature:: In N,N-dimethyl-formamide; for 6h; Heating;
DOI:10.1039/P19850000399

Reference yield:

: 23938-71-8
2-propionyl-γ-butyrolactone

: 96890-24-3
3-(2-ethyl-1,3-dioxolan-2-yl)propyltriphenylphosphonium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / 48percent HBr / toluene / 0.75 h

2: 2.) 1M NaI / 1.) CH₃CN, 36 h, reflux 2.) CH₂Cl₂

3: 92 percent / molecular sieve (4 Angstroem), p-toluenesulfonic acid / CHCl₃ / 36 h

With 4 A molecular sieve; hydrogen bromide; toluene-4-sulfonic acid; sodium iodide; In chloroform; toluene;
DOI:10.1016/S0040-4020(01)86399-7