2-[4-([3-tert-butoxycarbonylaminophenyl]amino)-6-chloro[1,3,5]-triazine-2-ylamino]ethanol

Base Information

• Chemical Name: 2-[4-([3-tert-butoxycarbonylaminophenyl]amino)-6-chloro[1,3,5]-triazine-2-ylamino]ethanol
• CAS No.: 1192801-06-1
• Molecular Formula: C₁₆H₂₁ClN₆O₃
• Molecular Weight: 380.834

Synonyms:2-[4-([3-tert-butoxycarbonylaminophenyl]amino)-6-chloro[1,3,5]-triazine-2-ylamino]ethanol

Chemical Property of 2-[4-([3-tert-butoxycarbonylaminophenyl]amino)-6-chloro[1,3,5]-triazine-2-ylamino]ethanol

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Technology Process of 2-[4-([3-tert-butoxycarbonylaminophenyl]amino)-6-chloro[1,3,5]-triazine-2-ylamino]ethanol

There total 1 articles about 2-[4-([3-tert-butoxycarbonylaminophenyl]amino)-6-chloro[1,3,5]-triazine-2-ylamino]ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

ethanolamine (141-43-5) + 2-[3-(tert-butoxycarbonylamino)phenylamino]-4,6-dichloro-1,3,5-triazine (537049-05-1) → 2-[4-([3-tert-butoxycarbonylaminophenyl]amino)-6-chloro[1,3,5]-triazine-2-ylamino]ethanol (1192801-06-1)

Guidance literature:

With sodium hydrogencarbonate; In tetrahydrofuran; water; acetone; at 20 ℃;

DOI:10.1021/jm901403r

Reference yield: 83.0%

2-[4-([3-tert-butoxycarbonylaminophenyl]amino)-6-chloro[1,3,5]-triazine-2-ylamino]ethanol (1192801-06-1) + 4-(2-aminoethyl)aniline dihydrochloride (13078-82-5,29968-79-4,102606-30-4) → 2-[4-[2-[4-aminophenyl]ethylamino]-6-([3-tert-butoxycarbonylaminophenyl]amino)[1,3,5]triazine-2-ylamino]ethanol (1192801-07-2)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In water; acetonitrile; at 60 ℃; for 48h; Inert atmosphere;

DOI:10.1021/op900202b

Reference yield: 81.0%

p-Aminophenethylamine (13472-00-9) + 2-[4-([3-tert-butoxycarbonylaminophenyl]amino)-6-chloro[1,3,5]-triazine-2-ylamino]ethanol (1192801-06-1) → 2-[4-[2-[4-aminophenyl]ethylamino]-6-([3-tert-butoxycarbonylaminophenyl]amino)[1,3,5]triazine-2-ylamino]ethanol (1192801-07-2)

Guidance literature:

In tetrahydrofuran; at 60 ℃;

DOI:10.1021/jm901403r

upstream raw materials:

ethanolamine

2-[3-(tert-butoxycarbonylamino)phenylamino]-4,6-dichloro-1,3,5-triazine

Downstream raw materials:

2-[4-[2-[4-aminophenyl]ethylamino]-6-([3-tert-butoxycarbonylaminophenyl]amino)[1,3,5]triazine-2-ylamino]ethanol

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