Technology Process of (1-adamantyl)diazophenylmethane
There total 4 articles about (1-adamantyl)diazophenylmethane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
barium manganate; calcium oxide;
In
diethyl ether;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/jacs.0c02221
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: thionyl chloride / 2 h / 20 °C
2.1: magnesium / diethyl ether / 20 °C / Inert atmosphere; Reflux
2.2: 1.67 h / 20 °C / Cooling with ice; Reflux
2.3: 20 °C / Reflux
3.1: hydrazine hydrate / methanol / 24 h / Reflux
4.1: barium manganate; calcium oxide / diethyl ether / 1 h / 20 °C / Inert atmosphere
With
thionyl chloride; barium manganate; hydrazine hydrate; magnesium; calcium oxide;
In
methanol; diethyl ether;
DOI:10.1021/jacs.0c02221
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: magnesium / diethyl ether / 20 °C / Inert atmosphere; Reflux
1.2: 1.67 h / 20 °C / Cooling with ice; Reflux
1.3: 20 °C / Reflux
2.1: hydrazine hydrate / methanol / 24 h / Reflux
3.1: barium manganate; calcium oxide / diethyl ether / 1 h / 20 °C / Inert atmosphere
With
barium manganate; hydrazine hydrate; magnesium; calcium oxide;
In
methanol; diethyl ether;
DOI:10.1021/jacs.0c02221
