(1-adamantyl)diazophenylmethane

Base Information

Chemical Name:(1-adamantyl)diazophenylmethane
CAS No.:180515-91-7
Molecular Formula:C₁₇H₂₀N₂
Molecular Weight:252.359
Hs Code.:

Synonyms:(1-adamantyl)diazophenylmethane

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Chemical Property of (1-adamantyl)diazophenylmethane

Chemical Property:

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Technology Process of (1-adamantyl)diazophenylmethane

There total 4 articles about (1-adamantyl)diazophenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1-adamantyl phenyl ketone hydrazone

: 180515-91-7
(1-adamantyl)diazophenylmethane

Guidance literature:: With barium manganate; calcium oxide; In diethyl ether; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jacs.0c02221

Reference yield:

: 828-51-3
1-Adamantanecarboxylic acid

: 180515-91-7
(1-adamantyl)diazophenylmethane

Guidance literature:: Multi-step reaction with 4 steps

1.1: thionyl chloride / 2 h / 20 °C

2.1: magnesium / diethyl ether / 20 °C / Inert atmosphere; Reflux

2.2: 1.67 h / 20 °C / Cooling with ice; Reflux

2.3: 20 °C / Reflux

3.1: hydrazine hydrate / methanol / 24 h / Reflux

4.1: barium manganate; calcium oxide / diethyl ether / 1 h / 20 °C / Inert atmosphere

With thionyl chloride; barium manganate; hydrazine hydrate; magnesium; calcium oxide; In methanol; diethyl ether;
DOI:10.1021/jacs.0c02221

Reference yield:

: 2094-72-6
1-Adamantanecarbonyl chloride

: 180515-91-7
(1-adamantyl)diazophenylmethane

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium / diethyl ether / 20 °C / Inert atmosphere; Reflux

1.2: 1.67 h / 20 °C / Cooling with ice; Reflux

1.3: 20 °C / Reflux

2.1: hydrazine hydrate / methanol / 24 h / Reflux

3.1: barium manganate; calcium oxide / diethyl ether / 1 h / 20 °C / Inert atmosphere

With barium manganate; hydrazine hydrate; magnesium; calcium oxide; In methanol; diethyl ether;
DOI:10.1021/jacs.0c02221